phenyl 2,3,4-tri-O-benzyl-6-O-[bis(phenoxy)phosphoryl]-1-thio-α-D-altropyranoside

Base Information

Chemical Name:phenyl 2,3,4-tri-O-benzyl-6-O-[bis(phenoxy)phosphoryl]-1-thio-α-D-altropyranoside
CAS No.:1606161-59-4
Molecular Formula:C₄₅H₄₃O₈PS
Molecular Weight:774.871
Hs Code.:

Synonyms:phenyl 2,3,4-tri-O-benzyl-6-O-[bis(phenoxy)phosphoryl]-1-thio-α-D-altropyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 2,3,4-tri-O-benzyl-6-O-[bis(phenoxy)phosphoryl]-1-thio-α-D-altropyranoside

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Technology Process of phenyl 2,3,4-tri-O-benzyl-6-O-[bis(phenoxy)phosphoryl]-1-thio-α-D-altropyranoside

There total 2 articles about phenyl 2,3,4-tri-O-benzyl-6-O-[bis(phenoxy)phosphoryl]-1-thio-α-D-altropyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1290177-30-8
phenyl 2 ,3,4-tri-O-benzyl-1-thio-α-D-altropyranoside

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 1606161-59-4
phenyl 2,3,4-tri-O-benzyl-6-O-[bis(phenoxy)phosphoryl]-1-thio-α-D-altropyranoside

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 1606161-57-2
phenyl 2,3,4-tri-O-benzyl-1-thio-6-O-triisopropylsilyl-α-D-altropyranoside

: 1606161-59-4
phenyl 2,3,4-tri-O-benzyl-6-O-[bis(phenoxy)phosphoryl]-1-thio-α-D-altropyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

With dmap; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; dichloromethane;