6-(6-amino-hexanoylamino)-hexanoic acid-(4-nitro-phenyl ester); hydrobromide

Base Information

Chemical Name:6-(6-amino-hexanoylamino)-hexanoic acid-(4-nitro-phenyl ester); hydrobromide
CAS No.:109565-05-1
Molecular Formula:BrH*C₁₈H₂₇N₃O₅
Molecular Weight:446.341
Hs Code.:

Synonyms:6-(6-amino-hexanoylamino)-hexanoic acid-(4-nitro-phenyl ester); hydrobromide

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Chemical Property of 6-(6-amino-hexanoylamino)-hexanoic acid-(4-nitro-phenyl ester); hydrobromide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of 6-(6-amino-hexanoylamino)-hexanoic acid-(4-nitro-phenyl ester); hydrobromide

There total 6 articles about 6-(6-amino-hexanoylamino)-hexanoic acid-(4-nitro-phenyl ester); hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1947-00-8
6-(benzyloxycarbonylamino)hexanoic acid

: 109565-05-1
6-(6-amino-hexanoylamino)-hexanoic acid-(4-nitro-phenyl ester); hydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: DCC / dioxane / 24 h / 0 °C

2: aq. NaHCO₃ / 1,2-dimethoxy-ethane / 5 h / 20 °C

3: 90 percent / DCC / dimethylformamide / 3 h / 0 - 20 °C

4: 33percent HBr / acetic acid / 2 h / 20 °C

With hydrogen bromide; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In 1,4-dioxane; 1,2-dimethoxyethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1007/BF00473947

Reference yield:

: 49701-55-5
13-benzyloxycarbonylamino-8-oxo-7-azatridecanoic acid

: 109565-05-1
6-(6-amino-hexanoylamino)-hexanoic acid-(4-nitro-phenyl ester); hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / DCC / dimethylformamide / 3 h / 0 - 20 °C

2: 33percent HBr / acetic acid / 2 h / 20 °C

With hydrogen bromide; dicyclohexyl-carbodiimide; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1007/BF00473947

Reference yield:

: 60-32-2,93208-38-9
6-aminohexanoic acid

: 109565-05-1
6-(6-amino-hexanoylamino)-hexanoic acid-(4-nitro-phenyl ester); hydrobromide

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / 4 M NaOH / 4 h / 0 - 20 °C

2: DCC / dioxane / 24 h / 0 °C

3: aq. NaHCO₃ / 1,2-dimethoxy-ethane / 5 h / 20 °C

4: 90 percent / DCC / dimethylformamide / 3 h / 0 - 20 °C

5: 33percent HBr / acetic acid / 2 h / 20 °C

With sodium hydroxide; hydrogen bromide; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In 1,4-dioxane; 1,2-dimethoxyethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1007/BF00473947