1,2-bis[6-(4-hydroxyphenyl)-2-methylbenzothiophen-3-yl]perfluorocyclopentene

Base Information

Chemical Name:1,2-bis[6-(4-hydroxyphenyl)-2-methylbenzothiophen-3-yl]perfluorocyclopentene
CAS No.:787587-08-0
Molecular Formula:C₃₅H₂₂F₆O₂S₂
Molecular Weight:652.681
Hs Code.:

Synonyms:1,2-bis[6-(4-hydroxyphenyl)-2-methylbenzothiophen-3-yl]perfluorocyclopentene

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Chemical Property of 1,2-bis[6-(4-hydroxyphenyl)-2-methylbenzothiophen-3-yl]perfluorocyclopentene

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Technology Process of 1,2-bis[6-(4-hydroxyphenyl)-2-methylbenzothiophen-3-yl]perfluorocyclopentene

There total 3 articles about 1,2-bis[6-(4-hydroxyphenyl)-2-methylbenzothiophen-3-yl]perfluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 787587-07-9
1,2-bis[6-(4-methoxyphenyl)-2-methylbenzothiophen-3-yl]perfluorocyclopentene

: 787587-08-0
1,2-bis[6-(4-hydroxyphenyl)-2-methylbenzothiophen-3-yl]perfluorocyclopentene

Guidance literature:: With boron tribromide; In n-heptane; dichloromethane; at -78 ℃; for 6h;
DOI:10.1039/b403188a

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 787587-08-0
1,2-bis[6-(4-hydroxyphenyl)-2-methylbenzothiophen-3-yl]perfluorocyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / Pd(Ph₃P)4; aq. Na₂CO₃ / tetrahydrofuran / 24 h / Heating

2: 84 percent / BBr₃ / heptane; CH₂Cl₂ / 6 h / -78 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; sodium carbonate; In tetrahydrofuran; n-heptane; dichloromethane; 1: Suzuki-Miyaura cross-coupling;
DOI:10.1039/b403188a

Reference yield:

: 167890-07-5
1,2-bis(6-iodo-2-methylbenzothiophen-3-yl)-3,3,4,4,5,5-hexafluorocyclopentene

: 787587-08-0
1,2-bis[6-(4-hydroxyphenyl)-2-methylbenzothiophen-3-yl]perfluorocyclopentene

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / Pd(Ph₃P)4; aq. Na₂CO₃ / tetrahydrofuran / 24 h / Heating

2: 84 percent / BBr₃ / heptane; CH₂Cl₂ / 6 h / -78 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; sodium carbonate; In tetrahydrofuran; n-heptane; dichloromethane; 1: Suzuki-Miyaura cross-coupling;
DOI:10.1039/b403188a