2-(3-(N,N-bis-tert-butoxycarbonylguanidino)benzoyl)-amino acetic acid benzyl ester

Base Information

Chemical Name:2-(3-(N,N-bis-tert-butoxycarbonylguanidino)benzoyl)-amino acetic acid benzyl ester
CAS No.:1448718-81-7
Molecular Formula:C₂₇H₃₄N₄O₇
Molecular Weight:526.59
Hs Code.:

Synonyms:2-(3-(N,N-bis-tert-butoxycarbonylguanidino)benzoyl)-amino acetic acid benzyl ester

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Chemical Property of 2-(3-(N,N-bis-tert-butoxycarbonylguanidino)benzoyl)-amino acetic acid benzyl ester

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Technology Process of 2-(3-(N,N-bis-tert-butoxycarbonylguanidino)benzoyl)-amino acetic acid benzyl ester

There total 4 articles about 2-(3-(N,N-bis-tert-butoxycarbonylguanidino)benzoyl)-amino acetic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.3%

: 197719-74-7
3-(N,N-bis-tert-butoxycarbonylguanidino)-benzoic acid

: 1448718-81-7
2-(3-(N,N-bis-tert-butoxycarbonylguanidino)benzoyl)-amino acetic acid benzyl ester

Guidance literature:: 3-(N,N-bis-tert-butoxycarbonylguanidino)-benzoic acid; With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; In tetrahydrofuran; at 20 ℃; for 2h;

With 4-methyl-morpholine; glycine benzyl ester p-toluenesulfonic acid salt; In tetrahydrofuran; at 20 ℃; for 36h;

Reference yield: 79.3%

: 197719-74-7
3-(N,N-bis-tert-butoxycarbonylguanidino)-benzoic acid

: 1738-76-7
glycine benzyl ester p-toluenesulfonic acid salt

: 1448718-81-7
2-(3-(N,N-bis-tert-butoxycarbonylguanidino)benzoyl)-amino acetic acid benzyl ester

Guidance literature:: 3-(N,N-bis-tert-butoxycarbonylguanidino)-benzoic acid; With 4-methyl-morpholine; 2-chloro-4,6-dimethoxytriazine; In tetrahydrofuran; at 20 ℃; for 2h;

glycine benzyl ester p-toluenesulfonic acid salt; With 4-methyl-morpholine; In tetrahydrofuran; at 20 ℃; for 36h;

Reference yield:

: 99-05-8,159139-79-4
meta-aminobenzoic acid

: 1448718-81-7
2-(3-(N,N-bis-tert-butoxycarbonylguanidino)benzoyl)-amino acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: mercury(II) diacetate; pyridine / N,N-dimethyl-formamide; 1,2-dichloro-ethane / 5 h / 20 °C

2.1: 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; 4-methyl-morpholine / tetrahydrofuran / 2 h / 20 °C

2.2: 36 h / 20 °C

With 4-methyl-morpholine; pyridine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; mercury(II) diacetate; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide;