1-methyl-1-phenyl-6-<1-(2-pyridinyl-ethylidene)amino>-2,5-dithiobiurea

Base Information

• Chemical Name: 1-methyl-1-phenyl-6-<1-(2-pyridinyl-ethylidene)amino>-2,5-dithiobiurea
• CAS No.: 88324-31-6
• Molecular Formula: C₁₆H₁₈N₆S₂
• Molecular Weight: 358.491
• Mol file: 88324-31-6.mol

Synonyms:1-methyl-1-phenyl-6-<1-(2-pyridinyl-ethylidene)amino>-2,5-dithiobiurea

Chemical Property of 1-methyl-1-phenyl-6-<1-(2-pyridinyl-ethylidene)amino>-2,5-dithiobiurea

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-methyl-1-phenyl-6-<1-(2-pyridinyl-ethylidene)amino>-2,5-dithiobiurea

There total 3 articles about 1-methyl-1-phenyl-6-<1-(2-pyridinyl-ethylidene)amino>-2,5-dithiobiurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2-acetylpyridine (1122-62-9) + 4-methyl-4-phenyl-3-thiosemicarbazide (21076-11-9) → 1-methyl-1-phenyl-6-<1-(2-pyridinyl-ethylidene)amino>-2,5-dithiobiurea (88324-31-6)

Guidance literature:

In acetonitrile; at 60 ℃; for 0.75h;

Reference yield:

N-methylaniline (100-61-8) → 1-methyl-1-phenyl-6-<1-(2-pyridinyl-ethylidene)amino>-2,5-dithiobiurea (88324-31-6)

Guidance literature:

Multi-step reaction with 2 steps

2: 89 percent / acetonitrile / 0.75 h / 60 °C

In acetonitrile;

Reference yield:

2-(N-Phenyl-N-methyl-thiocarbamoylthio)acetic Acid (20069-27-6) → 1-methyl-1-phenyl-6-<1-(2-pyridinyl-ethylidene)amino>-2,5-dithiobiurea (88324-31-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / NH₂-NH₂*H₂O / H₂O / 0.42 h / 85 °C

2: 89 percent / acetonitrile / 0.75 h / 60 °C

With hydrazine hydrate; In water; acetonitrile;

upstream raw materials:

2-acetylpyridine

4-methyl-4-phenyl-3-thiosemicarbazide

N-methylaniline

2-(N-Phenyl-N-methyl-thiocarbamoylthio)acetic Acid

Downstream raw materials:

3-methyl-5--1-<1-(2-pyridinyl)ethylidene>-3-thioisocarbohydrazide