tert-Butyl 3-(N-{[N-{2-[(tert-Butyl)oxycarbonyl]ethyl}-N-({N-[3-(5-{5-[5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl](1,2,3,4-tetraazolyl)}-pentanoylamino)propyl]carbamoyl}methyl)carbamoyl]methyl}-(fluoren-9-ylmethoxy)carbonylamino)propanoate

Base Information

Chemical Name:tert-Butyl 3-(N-{[N-{2-[(tert-Butyl)oxycarbonyl]ethyl}-N-({N-[3-(5-{5-[5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl](1,2,3,4-tetraazolyl)}-pentanoylamino)propyl]carbamoyl}methyl)carbamoyl]methyl}-(fluoren-9-ylmethoxy)carbonylamino)propanoate
CAS No.:556063-12-8
Molecular Formula:C₆₆H₈₃N₉O₁₀
Molecular Weight:1162.44
Hs Code.:

tert-Butyl 3-(N-{[N-{2-[(tert-Butyl)oxycarbonyl]ethyl}-N-({N-[3-(5-{5-[5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl](1,2,3,4-tetraazolyl)}-pentanoylamino)propyl]carbamoyl}methyl)carbamoyl]methyl}-(fluoren-9-ylmethoxy)carbonylamino)propanoate

Synonyms:tert-Butyl 3-(N-{[N-{2-[(tert-Butyl)oxycarbonyl]ethyl}-N-({N-[3-(5-{5-[5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl](1,2,3,4-tetraazolyl)}-pentanoylamino)propyl]carbamoyl}methyl)carbamoyl]methyl}-(fluoren-9-ylmethoxy)carbonylamino)propanoate

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Chemical Property of tert-Butyl 3-(N-{[N-{2-[(tert-Butyl)oxycarbonyl]ethyl}-N-({N-[3-(5-{5-[5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl](1,2,3,4-tetraazolyl)}-pentanoylamino)propyl]carbamoyl}methyl)carbamoyl]methyl}-(fluoren-9-ylmethoxy)carbonylamino)propanoate

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Technology Process of tert-Butyl 3-(N-{[N-{2-[(tert-Butyl)oxycarbonyl]ethyl}-N-({N-[3-(5-{5-[5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl](1,2,3,4-tetraazolyl)}-pentanoylamino)propyl]carbamoyl}methyl)carbamoyl]methyl}-(fluoren-9-ylmethoxy)carbonylamino)propanoate

There total 3 articles about tert-Butyl 3-(N-{[N-{2-[(tert-Butyl)oxycarbonyl]ethyl}-N-({N-[3-(5-{5-[5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl](1,2,3,4-tetraazolyl)}-pentanoylamino)propyl]carbamoyl}methyl)carbamoyl]methyl}-(fluoren-9-ylmethoxy)carbonylamino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 556063-11-7
N-{3-[(tert-Butoxy)carbonylamino]-propyl}-5-{5-[5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl](1,2,3,4-tetraazolyl)}pentanamide

: 174799-89-4
N-fluorenylmethoxycarbonyl-N′-carboxymethyl-β-alanine-t-butyl ester

: 556063-12-8
tert-Butyl 3-(N-{[N-{2-[(tert-Butyl)oxycarbonyl]ethyl}-N-({N-[3-(5-{5-[5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl](1,2,3,4-tetraazolyl)}-pentanoylamino)propyl]carbamoyl}methyl)carbamoyl]methyl}-(fluoren-9-ylmethoxy)carbonylamino)propanoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In piperidine; quinoclamine; water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; ethyl acetate; N,N-dimethyl-formamide; trifluoroacetic acid;

Reference yield:

: 206265-90-9
5-(5-(5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl)-1,2,3,4-tetrazoyl)pentanoic acid

: 556063-12-8
tert-Butyl 3-(N-{[N-{2-[(tert-Butyl)oxycarbonyl]ethyl}-N-({N-[3-(5-{5-[5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl](1,2,3,4-tetraazolyl)}-pentanoylamino)propyl]carbamoyl}methyl)carbamoyl]methyl}-(fluoren-9-ylmethoxy)carbonylamino)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / chloroform; N,N-dimethyl-formamide

2: N-ethyl-N,N-diisopropylamine / piperidine; quinoclamine; water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; ethyl acetate; N,N-dimethyl-formamide; trifluoroacetic acid

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In piperidine; chloroform; quinoclamine; water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; ethyl acetate; N,N-dimethyl-formamide; trifluoroacetic acid;

Reference yield:

: 206265-82-9
ethyl 5-(5-(5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl)-1,2,3,4-tetrazolyl)pentanoate

: 556063-12-8
tert-Butyl 3-(N-{[N-{2-[(tert-Butyl)oxycarbonyl]ethyl}-N-({N-[3-(5-{5-[5-(4,6-diphenyl(2-pyridyloxy))-1,1-dimethylpentyl](1,2,3,4-tetraazolyl)}-pentanoylamino)propyl]carbamoyl}methyl)carbamoyl]methyl}-(fluoren-9-ylmethoxy)carbonylamino)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: LiOH / tetrahydrofuran

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / chloroform; N,N-dimethyl-formamide

3: N-ethyl-N,N-diisopropylamine / piperidine; quinoclamine; water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; ethyl acetate; N,N-dimethyl-formamide; trifluoroacetic acid

With LiOH; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; piperidine; chloroform; quinoclamine; water; 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; ethyl acetate; N,N-dimethyl-formamide; trifluoroacetic acid;