C₃₅H₄₄N₂OSi

Base Information

Chemical Name:C₃₅H₄₄N₂OSi
CAS No.:1275592-92-1
Molecular Formula:C₃₅H₄₄N₂OSi
Molecular Weight:536.833
Hs Code.:

C<sub>35</sub>H<sub>44</sub>N<sub>2</sub>OSi

Synonyms:C₃₅H₄₄N₂OSi

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Chemical Property of C₃₅H₄₄N₂OSi

Chemical Property:

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Technology Process of C₃₅H₄₄N₂OSi

There total 11 articles about C₃₅H₄₄N₂OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1275592-91-0
(R)-2-{(4aR,12aS)-7-(2-tert-butyldiphenylsilyloxyethyl)-4a-ethyl-1,2,3,4,4a,5,6,12a-octahydroindolo[1,2-a][1,8]naphthyridin-1-yl}-2-phenylethanol

: 1275592-92-1
C₃₅H₄₄N₂OSi

Guidance literature:: With hydrogen; palladium(II) hydroxide; In 1,4-dioxane; propan-1-ol; at 20 ℃; for 11h; under 760.051 Torr;
DOI:10.1021/ol200320z

Reference yield:

: 161117-84-6
tert-butyl 2-iodophenylcarbamate

: 1275592-92-1
C₃₅H₄₄N₂OSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(l) iodide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; tetrabutyl-ammonium chloride / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2.1: Hoveyda-Grubbs catalyst second generation / 5,5-dimethyl-1,3-cyclohexadiene / 3 h / 140 °C / Inert atmosphere

3.1: 5% Pd(II)/C(eggshell); hydrogen / ethyl acetate / 27 h / 20 °C / 760.05 Torr

4.1: sodium hydride / diethyl ether; oil / 0.5 h / 0 °C / Inert atmosphere

4.2: 0 - 20 °C / Inert atmosphere

5.1: hydrogen; palladium(II) hydroxide / 1,4-dioxane; propan-1-ol / 11 h / 20 °C / 760.05 Torr

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; Hoveyda-Grubbs catalyst second generation; trifuran-2-yl-phosphane; 5% Pd(II)/C(eggshell); tetrabutyl-ammonium chloride; hydrogen; palladium(II) hydroxide; sodium hydride; In 1,4-dioxane; propan-1-ol; 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; ethyl acetate; N,N-dimethyl-formamide; oil; 1.1: Stille coupling;
DOI:10.1021/ol200320z

Reference yield:

: 1275592-79-4
1-benzyloxy-6-tert-butyldiphenylsilyloxy-4-tributylstannylhexa-2,3-diene

: 1275592-92-1
C₃₅H₄₄N₂OSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(l) iodide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; trifuran-2-yl-phosphane; tetrabutyl-ammonium chloride / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

2.1: Hoveyda-Grubbs catalyst second generation / 5,5-dimethyl-1,3-cyclohexadiene / 3 h / 140 °C / Inert atmosphere

3.1: 5% Pd(II)/C(eggshell); hydrogen / ethyl acetate / 27 h / 20 °C / 760.05 Torr

4.1: sodium hydride / diethyl ether; oil / 0.5 h / 0 °C / Inert atmosphere

4.2: 0 - 20 °C / Inert atmosphere

5.1: hydrogen; palladium(II) hydroxide / 1,4-dioxane; propan-1-ol / 11 h / 20 °C / 760.05 Torr

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; copper(l) iodide; Hoveyda-Grubbs catalyst second generation; trifuran-2-yl-phosphane; 5% Pd(II)/C(eggshell); tetrabutyl-ammonium chloride; hydrogen; palladium(II) hydroxide; sodium hydride; In 1,4-dioxane; propan-1-ol; 5,5-dimethyl-1,3-cyclohexadiene; diethyl ether; ethyl acetate; N,N-dimethyl-formamide; oil; 1.1: Stille coupling;
DOI:10.1021/ol200320z