2-[5-chloro-2-(2-methoxyphenyl)-1H-benzo[d]imidazol-1-yl]-N,N-diethylethanamine

Base Information

Chemical Name:2-[5-chloro-2-(2-methoxyphenyl)-1H-benzo[d]imidazol-1-yl]-N,N-diethylethanamine
CAS No.:1415488-80-0
Molecular Formula:C₂₀H₂₄ClN₃O
Molecular Weight:357.883
Hs Code.:

Synonyms:2-[5-chloro-2-(2-methoxyphenyl)-1H-benzo[d]imidazol-1-yl]-N,N-diethylethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[5-chloro-2-(2-methoxyphenyl)-1H-benzo[d]imidazol-1-yl]-N,N-diethylethanamine

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Technology Process of 2-[5-chloro-2-(2-methoxyphenyl)-1H-benzo[d]imidazol-1-yl]-N,N-diethylethanamine

There total 2 articles about 2-[5-chloro-2-(2-methoxyphenyl)-1H-benzo[d]imidazol-1-yl]-N,N-diethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.3%

: 4926-56-1
N¹-(4-chloro-2-nitrophenyl)-N²,N²-dimethylethane-1,2-diamine

: 135-02-4
ortho-anisaldehyde

: 1415488-80-0
2-[5-chloro-2-(2-methoxyphenyl)-1H-benzo[d]imidazol-1-yl]-N,N-diethylethanamine

Guidance literature:: With sodium dithionite; In ethanol; water; at 90 ℃; for 5h;
DOI:10.1021/ml300282t

Reference yield:

: 89-61-2
2,5-dichloronitrobenzene

: 1415488-80-0
2-[5-chloro-2-(2-methoxyphenyl)-1H-benzo[d]imidazol-1-yl]-N,N-diethylethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 80 °C

2: sodium dithionite / ethanol; water / 5 h / 90 °C

With sodium dithionite; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ml300282t