EtO₂CCHC(Me)(o-MeC₆H₄)

Base Information

Chemical Name:EtO₂CCHC(Me)(o-MeC₆H₄)
CAS No.:100994-06-7
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:

EtO<sub>2</sub>CCHC(Me)(o-MeC<sub>6</sub>H<sub>4</sub>)

Synonyms:EtO₂CCHC(Me)(o-MeC₆H₄)

Suppliers and Price of EtO₂CCHC(Me)(o-MeC₆H₄)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of EtO₂CCHC(Me)(o-MeC₆H₄)

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Technology Process of EtO₂CCHC(Me)(o-MeC₆H₄)

There total 10 articles about EtO₂CCHC(Me)(o-MeC₆H₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 52883-70-2
ethyl (E)-3-(pivaloyloxy)but-2-enoate

: 84109-17-1
2-methylphenylzinc chloride

: 100994-06-7
(E)-ethyl 3-(2-methylphenyl)-but-2-enoate

Guidance literature:: With bis(tricyclohexylphosphine)nickel(II) dichloride; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; at 25 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c7ob02947k

Reference yield: 80.0%

: 4341-76-8
Ethyl 2-butynoate

: 16419-60-6
2-Methylphenylboronic acid

: 100994-06-7
(E)-ethyl 3-(2-methylphenyl)-but-2-enoate

Guidance literature:: With water; palladium diacetate; triethylphosphonium tetrafluoroborate; caesium carbonate; In toluene; at 23 ℃; for 18h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2009.08.029

Reference yield: 64.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 577-16-2,122382-54-1
2-Methylacetophenone

: 100994-06-7
(E)-ethyl 3-(2-methylphenyl)-but-2-enoate

Guidance literature:: diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

2-Methylacetophenone; In tetrahydrofuran; mineral oil; at 40 ℃; for 48h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c8cc09853k