4,4'-bis-ethylsulfanyl-2,2'-diphenyl-N₅,N₅'-bis-(4-tert.-butyl-phenyl)-4H,4'H-[4,4']biimidazolyl-5,5'-diamine

Base Information

• Chemical Name: 4,4'-bis-ethylsulfanyl-2,2'-diphenyl-N₅,N₅'-bis-(4-tert.-butyl-phenyl)-4H,4'H-[4,4']biimidazolyl-5,5'-diamine
• CAS No.: 328378-57-0
• Molecular Formula: C₄₂H₄₈N₆S₂
• Molecular Weight: 701.015

Synonyms:4,4'-bis-ethylsulfanyl-2,2'-diphenyl-N₅,N₅'-bis-(4-tert.-butyl-phenyl)-4H,4'H-[4,4']biimidazolyl-5,5'-diamine

Chemical Property of 4,4'-bis-ethylsulfanyl-2,2'-diphenyl-N₅,N₅'-bis-(4-tert.-butyl-phenyl)-4H,4'H-[4,4']biimidazolyl-5,5'-diamine

Chemical Property:

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Technology Process of 4,4'-bis-ethylsulfanyl-2,2'-diphenyl-N₅,N₅'-bis-(4-tert.-butyl-phenyl)-4H,4'H-[4,4']biimidazolyl-5,5'-diamine

There total 1 articles about 4,4'-bis-ethylsulfanyl-2,2'-diphenyl-N₅,N₅'-bis-(4-tert.-butyl-phenyl)-4H,4'H-[4,4']biimidazolyl-5,5'-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

ethanethiol (75-08-1) + (4-tert-butyl-phenyl)-[5-(4-tert-butyl-phenylimino)-2-phenyl-5H-imidazol-4-yl]-amine → 4,4'-bis-ethylsulfanyl-2,2'-diphenyl-N5,N5'-bis-(4-tert.-butyl-phenyl)-4H,4'H-[4,4']biimidazolyl-5,5'-diamine (328378-57-0)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; at 50 ℃;

DOI:10.1007/s007060070026

Reference yield: 47.0%

4,4'-bis-ethylsulfanyl-2,2'-diphenyl-N5,N5'-bis-(4-tert.-butyl-phenyl)-4H,4'H-[4,4']biimidazolyl-5,5'-diamine (328378-57-0) → 5-(4-tert.-butyl-phenylamino)-2-phenyl-imidazol-4-one

Guidance literature:

With tetraphenylporphyrine; oxygen; In dichloromethane; at -20 ℃; for 3h; Irradiation;

DOI:10.1007/s007060070026

Reference yield: 41.0%

4,4'-bis-ethylsulfanyl-2,2'-diphenyl-N5,N5'-bis-(4-tert.-butyl-phenyl)-4H,4'H-[4,4']biimidazolyl-5,5'-diamine (328378-57-0) → 2,6-bis-phenyl-4,8-bis-(4-tert.-butylphenylamino)-1,3,5,7-tetraazafulvalene

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In toluene; Heating;

DOI:10.1007/s007060070026

upstream raw materials:

ethanethiol

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