C₁₆H₁₄N₂

Base Information

Chemical Name:C₁₆H₁₄N₂
CAS No.:1375062-48-8
Molecular Formula:C₁₆H₁₄N₂
Molecular Weight:234.301
Hs Code.:

C<sub>16</sub>H<sub>14</sub>N<sub>2</sub>

Synonyms:C₁₆H₁₄N₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₄N₂

Chemical Property:

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Technology Process of C₁₆H₁₄N₂

There total 3 articles about C₁₆H₁₄N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 877-42-9
6-Bromo-2-methyl-quinoline

: 615-36-1
2-bromoaniline

: 1375062-48-8
C₁₆H₁₄N₂

Guidance literature:: 6-Bromo-2-methyl-quinoline; With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; bis(pinacol)diborane; In toluene; at 90 ℃; for 18h; Inert atmosphere;

2-bromoaniline; With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; water; tricyclohexylphosphine; In 1,4-dioxane; at 100 ℃; for 17h; Inert atmosphere;
DOI:10.1021/ja302283s

Reference yield:

: 877-42-9
6-Bromo-2-methyl-quinoline

: 1375062-48-8
C₁₆H₁₄N₂

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / toluene / 18 h / 90 °C / Inert atmosphere

2: potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine / 1,4-dioxane; water / 17 h / 100 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium acetate; tricyclohexylphosphine; In 1,4-dioxane; water; toluene; 1: |Miyaura Borylation Reaction / 2: |Suzuki Coupling;

Reference yield:

: 1022090-86-3
2-methyl-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-quinoline

: 615-36-1
2-bromoaniline

: 1375062-48-8
C₁₆H₁₄N₂

Guidance literature:: With potassium phosphate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tricyclohexylphosphine; In 1,4-dioxane; water; at 100 ℃; for 17h; Inert atmosphere;