2-thioanisyldichlorophosphine

Base Information

Chemical Name:2-thioanisyldichlorophosphine
CAS No.:253686-37-2
Molecular Formula:C₇H₇Cl₂PS
Molecular Weight:225.078
Hs Code.:

Synonyms:2-thioanisyldichlorophosphine

Suppliers and Price of 2-thioanisyldichlorophosphine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-thioanisyldichlorophosphine

Chemical Property:

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Technology Process of 2-thioanisyldichlorophosphine

There total 1 articles about 2-thioanisyldichlorophosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.3%

: 19614-16-5
2-bromo-1-(methylsulfanyl)benzene

: 253686-37-2
2-thioanisyldichlorophosphine

Guidance literature:: 2-bromo-1-(methylsulfanyl)benzene; With n-butyllithium; In diethyl ether; hexane; at 0 ℃; for 2h;

With zinc(II) chloride; In diethyl ether; hexane; at 20 ℃; for 2h;

With phosphorus trichloride; In diethyl ether; hexane; for 40h; Heating;
DOI:10.1016/S0022-328X(99)00711-1

Reference yield: 64.3%

: 1564-64-3
9-Bromoanthracene

: 253686-37-2
2-thioanisyldichlorophosphine

: (2-thiomethylphenyl)bis(9-anthracenyl)phosphine

Guidance literature:: 9-Bromoanthracene; With n-butyllithium; In diethyl ether; hexane; at 0 ℃;

2-thioanisyldichlorophosphine; In diethyl ether; hexane; at 0 ℃;
DOI:10.1016/S0022-328X(99)00711-1

Reference yield: 62.2%

: 578-57-4
2-bromoanisole

: 253686-37-2
2-thioanisyldichlorophosphine

: 253686-42-9
(2-thiomethylphenyl)bis(2-methoxyphenyl)phosphine

Guidance literature:: 2-bromoanisole; With n-butyllithium; In diethyl ether; hexane; at 0 ℃;

2-thioanisyldichlorophosphine; In diethyl ether; hexane; at 0 ℃;
DOI:10.1016/S0022-328X(99)00711-1