1-(2-Benzenesulfinyl-ethyl)-7-(4-methoxy-benzenesulfonyl)-4,6,7,11c-tetrahydro-1H,3H-pyrido[3,2-c]carbazol-2-one

Base Information

Chemical Name:1-(2-Benzenesulfinyl-ethyl)-7-(4-methoxy-benzenesulfonyl)-4,6,7,11c-tetrahydro-1H,3H-pyrido[3,2-c]carbazol-2-one
CAS No.:82946-40-5
Molecular Formula:C₃₀H₂₈N₂O₅S₂
Molecular Weight:560.695
Hs Code.:

Synonyms:1-(2-Benzenesulfinyl-ethyl)-7-(4-methoxy-benzenesulfonyl)-4,6,7,11c-tetrahydro-1H,3H-pyrido[3,2-c]carbazol-2-one

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Chemical Property of 1-(2-Benzenesulfinyl-ethyl)-7-(4-methoxy-benzenesulfonyl)-4,6,7,11c-tetrahydro-1H,3H-pyrido[3,2-c]carbazol-2-one

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Technology Process of 1-(2-Benzenesulfinyl-ethyl)-7-(4-methoxy-benzenesulfonyl)-4,6,7,11c-tetrahydro-1H,3H-pyrido[3,2-c]carbazol-2-one

There total 7 articles about 1-(2-Benzenesulfinyl-ethyl)-7-(4-methoxy-benzenesulfonyl)-4,6,7,11c-tetrahydro-1H,3H-pyrido[3,2-c]carbazol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82946-38-1
1,3,4,6,7,11c-hexahydro-7-<(p-methoxyphenyl)sulfonyl>-1-<2-(phenylthio)ethyl>-2H-pyrido<3,2-c>carbazol-2-one

: 82946-40-5
1-(2-Benzenesulfinyl-ethyl)-7-(4-methoxy-benzenesulfonyl)-4,6,7,11c-tetrahydro-1H,3H-pyrido[3,2-c]carbazol-2-one

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; Yield given;
DOI:10.1021/ja00319a034

Reference yield:

: 82946-37-0
C₈H₁₀O₄

: 82946-40-5
1-(2-Benzenesulfinyl-ethyl)-7-(4-methoxy-benzenesulfonyl)-4,6,7,11c-tetrahydro-1H,3H-pyrido[3,2-c]carbazol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 31 percent / chlorobenzene / 2.5 h / 130 °C

2: m-chloroperbenzoic acid, NaHCO₃ / CH₂Cl₂

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chlorobenzene;
DOI:10.1039/c39820000613

Reference yield:

: 6089-09-4
4-pentynoic acid

: 82946-40-5
1-(2-Benzenesulfinyl-ethyl)-7-(4-methoxy-benzenesulfonyl)-4,6,7,11c-tetrahydro-1H,3H-pyrido[3,2-c]carbazol-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine

2: 37 percent / chlorobenzene / 0.5 h / 135 °C

3: 10percent aq. NaHCO₃, m-chloroperoxybenzoic acid / CH₂Cl₂ / 0 °C

With sodium hydrogencarbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chlorobenzene;
DOI:10.1021/ja00319a034