benzyl [36-13C]-1-[3-methyl-2-(4-methylpiperazin-1-yl)quinolin-4-yl]-1,33-dioxo-5,8,11,14,17,20,23,26,29-nonaoxa-2,32,34-triazahexatriacontan-36-oate

Base Information

Chemical Name:benzyl [36-13C]-1-[3-methyl-2-(4-methylpiperazin-1-yl)quinolin-4-yl]-1,33-dioxo-5,8,11,14,17,20,23,26,29-nonaoxa-2,32,34-triazahexatriacontan-36-oate
CAS No.:1309661-61-7
Molecular Formula:C₄₆H₇₀N₆O₁₃
Molecular Weight:916.083
Hs Code.:

Synonyms:benzyl [36-13C]-1-[3-methyl-2-(4-methylpiperazin-1-yl)quinolin-4-yl]-1,33-dioxo-5,8,11,14,17,20,23,26,29-nonaoxa-2,32,34-triazahexatriacontan-36-oate

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Chemical Property of benzyl [36-13C]-1-[3-methyl-2-(4-methylpiperazin-1-yl)quinolin-4-yl]-1,33-dioxo-5,8,11,14,17,20,23,26,29-nonaoxa-2,32,34-triazahexatriacontan-36-oate

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Technology Process of benzyl [36-13C]-1-[3-methyl-2-(4-methylpiperazin-1-yl)quinolin-4-yl]-1,33-dioxo-5,8,11,14,17,20,23,26,29-nonaoxa-2,32,34-triazahexatriacontan-36-oate

There total 5 articles about benzyl [36-13C]-1-[3-methyl-2-(4-methylpiperazin-1-yl)quinolin-4-yl]-1,33-dioxo-5,8,11,14,17,20,23,26,29-nonaoxa-2,32,34-triazahexatriacontan-36-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1202573-36-1
C₁₅⁽¹³⁾CH₁₄N₂O₆

: 1309661-59-3
N-(29-amino-3,6,9,12,15,18,21,24,27-nonaoxanonacosyl)-3-methyl-2-(4-methylpiperazin-1-yl)quinoline-4-carboxamide

: 1309661-61-7
benzyl [36-13C]-1-[3-methyl-2-(4-methylpiperazin-1-yl)quinolin-4-yl]-1,33-dioxo-5,8,11,14,17,20,23,26,29-nonaoxa-2,32,34-triazahexatriacontan-36-oate

Guidance literature:: In chloroform; at 20 ℃; for 72h; Inert atmosphere;
DOI:10.1021/ml2000388

Reference yield:

: 890091-43-7
tert-butyl 2-(2-(2-(2-(2-(2-(2-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethoxy)ethylcarbamate

: 1309661-61-7
benzyl [36-13C]-1-[3-methyl-2-(4-methylpiperazin-1-yl)quinolin-4-yl]-1,33-dioxo-5,8,11,14,17,20,23,26,29-nonaoxa-2,32,34-triazahexatriacontan-36-oate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 24 h / 20 °C

2.1: 4 h / 130 - 140 °C / Inert atmosphere

3.1: trifluoroacetic acid / 0.17 h / 20 °C

3.2: Saturated solution

4.1: chloroform / 72 h / 20 °C / Inert atmosphere

With triethylamine; trifluoroacetic acid; In dichloromethane; chloroform;
DOI:10.1021/ml2000388

Reference yield:

: 1309661-51-5
tert-butyl 1-(2-chloro-3-methylquinolin-4-yl)-1-oxo-5,8,11,14,17,20,23,26,29-nonaoxa-2-azahentriacontan-31-ylcarbamate

: 1309661-61-7
benzyl [36-13C]-1-[3-methyl-2-(4-methylpiperazin-1-yl)quinolin-4-yl]-1,33-dioxo-5,8,11,14,17,20,23,26,29-nonaoxa-2,32,34-triazahexatriacontan-36-oate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4 h / 130 - 140 °C / Inert atmosphere

2.1: trifluoroacetic acid / 0.17 h / 20 °C

2.2: Saturated solution

3.1: chloroform / 72 h / 20 °C / Inert atmosphere

With trifluoroacetic acid; In chloroform;
DOI:10.1021/ml2000388