2-methyl-2-phenyl-1,3-dithiolane 1,1,3,3-tetraoxide

Base Information

• Chemical Name: 2-methyl-2-phenyl-1,3-dithiolane 1,1,3,3-tetraoxide
• CAS No.: 6331-18-6
• Molecular Formula: C19H14N4O2S2
• Molecular Weight: 260.3299
• Mol file: 6331-18-6.mol

Synonyms:

Chemical Property of 2-methyl-2-phenyl-1,3-dithiolane 1,1,3,3-tetraoxide

Chemical Property:

• Vapor Pressure: 3.63E-12mmHg at 25°C
• Boiling Point: 564.1°C at 760 mmHg
• Flash Point: 397.6°C
• Density: 1.411g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-methyl-2-phenyl-1,3-dithiolane 1,1,3,3-tetraoxide

There total 2 articles about 2-methyl-2-phenyl-1,3-dithiolane 1,1,3,3-tetraoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-methyl-2-phenyl[1,3]dithiolane (5769-02-8) → 2-methyl-2-phenyl-1,3-dithiolane-1,1,3,3-tetraoxide (6331-18-6)

Guidance literature:

With dihydrogen peroxide; In acetic acid; at 60 - 70 ℃; for 8h;

DOI:10.1080/00397919308011151

Reference yield:

→ 2-methyl-2-phenyl-1,3-dithiolane-1,1,3,3-tetraoxide (6331-18-6)

Guidance literature:

Dithiaheterocyclus (1.4), H2O2;

Reference yield: 98.0%

2-methyl-2-phenyl-1,3-dithiolane-1,1,3,3-tetraoxide (6331-18-6) → 1-phenylethyl vinyl sulfone

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In ethanol; for 19h; Heating;

DOI:10.1080/00397919308011151

upstream raw materials:

2-methyl-2-phenyl[1,3]dithiolane

Refernces