3-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-4-methoxybenzoic acid

Base Information

Chemical Name:3-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-4-methoxybenzoic acid
CAS No.:1609477-33-9
Molecular Formula:C₂₅H₃₂O₇
Molecular Weight:444.525
Hs Code.:

Synonyms:3-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-4-methoxybenzoic acid

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Chemical Property of 3-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-4-methoxybenzoic acid

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Technology Process of 3-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-4-methoxybenzoic acid

There total 7 articles about 3-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-4-methoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609477-87-3
C₂₆H₃₄O₇

: 1609477-33-9
3-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-4-methoxybenzoic acid

Guidance literature:: C₂₆H₃₄O₇; With potassium hydroxide; In 1,4-dioxane; water; for 12h; Inert atmosphere;

With hydrogenchloride; In 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jm5000563

Reference yield:

: 6702-50-7
3-hydroxy-4-methoxybenzoate

: 1609477-33-9
3-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-4-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 6 h / 85 °C / Inert atmosphere

2: potassium carbonate; potassium iodide / acetonitrile / 0.25 h / 160 °C / Inert atmosphere; Microwave irradiation

3: potassium hydroxide / 1,4-dioxane; water / 12 h / Inert atmosphere

With potassium carbonate; potassium iodide; potassium hydroxide; In 1,4-dioxane; water; acetonitrile;
DOI:10.1021/jm5000563

Reference yield:

: 7065-46-5
3,3-dimethylbutanoic acid chloride

: 1609477-33-9
3-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-4-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate; potassium iodide / acetonitrile / 0.25 h / 160 °C / Inert atmosphere; Microwave irradiation

3: potassium hydroxide / 1,4-dioxane; water / 12 h / Inert atmosphere

With aluminum (III) chloride; potassium carbonate; potassium iodide; potassium hydroxide; In 1,4-dioxane; dichloromethane; water; acetonitrile; 1: |Friedel-Crafts Acylation;
DOI:10.1021/jm5000563