D-LYXOSE-DIETHYLDITHIOACETAL

Base Information

• Chemical Name: D-LYXOSE-DIETHYLDITHIOACETAL
• CAS No.: 6838-08-0
• Molecular Formula: C₉H₂₀O₄S₂
• Molecular Weight: 256.387
• Mol file: 6838-08-0.mol

Synonyms:(2R,3S,4S)-5,5-bis(ethylthio)pentane-1,2,3,4-tetraol

Chemical Property of D-LYXOSE-DIETHYLDITHIOACETAL

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

D-LYXOSE-DIETHYLDITHIOACETAL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of D-LYXOSE-DIETHYLDITHIOACETAL

There total 1 articles about D-LYXOSE-DIETHYLDITHIOACETAL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ DL-arabinose diethyl dithioacetal (1941-50-0,6838-08-0,7152-47-8,13263-74-6,22249-18-9,23259-79-2,43179-48-2,90820-06-7)

Guidance literature:

Reference yield: 92.0%

(2R,3S,4S)-5,5-bis(ethylthio)pentane-1,2,3,4-tetraol (6838-08-0) + benzyl bromide (100-39-0) → 2,3,4,5-tetra-O-benzyl diethyl dithioacetal D-lyxose (135983-28-7)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c8cc05523h

Reference yield: 81.0%

(2R,3S,4S)-5,5-bis(ethylthio)pentane-1,2,3,4-tetraol (6838-08-0) + trityl chloride (76-83-5) → (2S,3S,4R)-1,1-Bis-ethylsulfanyl-5-trityloxy-pentane-2,3,4-triol (96236-33-8)

Guidance literature:

DOI:10.1246/cl.1985.37

Downstream raw materials:

O²,O³,O⁴-triacetyl-O⁵-trityl-D-lyxose-diethyldithioacetal

O²,O³,O⁴-tribenzoyl-O⁵-trityl-D-lyxose-diethyldithioacetal

2,5-anhydro-D-lyxose diethyl dithioacetal

2,3,4,5-tetra-O-benzyl diethyl dithioacetal D-lyxose