4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)aniline

Base Information

Chemical Name:4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)aniline
CAS No.:1377617-63-4
Molecular Formula:C₂₃H₂₃N₃S₂
Molecular Weight:405.588
Hs Code.:

Synonyms:4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)aniline

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Chemical Property of 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)aniline

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Technology Process of 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)aniline

There total 2 articles about 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.9%

: 1377617-62-3
1-hexyl-2-(4-nitrophenyl)-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole

: 1377617-63-4
4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)aniline

Guidance literature:: 1-hexyl-2-(4-nitrophenyl)-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazole; With palladium 10% on activated carbon; In ethanol; for 0.333333h; Reflux;

With hydrazine hydrate; In ethanol; for 4h; Reflux;
DOI:10.1039/c2cc31131c

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 1377617-63-4
4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium acetate; acetic acid / 100 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 95 °C

2.2: 20 - 95 °C

3.1: palladium 10% on activated carbon / ethanol / 0.33 h / Reflux

3.2: 4 h / Reflux

With palladium 10% on activated carbon; ammonium acetate; potassium carbonate; acetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c2cc31131c