N-(tert-butoxycarbonyl)-O-(dibenzylphosphono)-L-tyrosyl p-nitro-benzyl ester

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-O-(dibenzylphosphono)-L-tyrosyl p-nitro-benzyl ester
CAS No.:92264-98-7
Molecular Formula:C₃₅H₃₇N₂O₁₀P
Molecular Weight:676.66
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-O-(dibenzylphosphono)-L-tyrosyl p-nitro-benzyl ester

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Chemical Property of N-(tert-butoxycarbonyl)-O-(dibenzylphosphono)-L-tyrosyl p-nitro-benzyl ester

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Technology Process of N-(tert-butoxycarbonyl)-O-(dibenzylphosphono)-L-tyrosyl p-nitro-benzyl ester

There total 5 articles about N-(tert-butoxycarbonyl)-O-(dibenzylphosphono)-L-tyrosyl p-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 538-37-4
dibenzyl phosphochloridate

: 92264-95-4
N-(tert-butoxycarbonyl)-L-tyrosyl p-nitrobenzyl ester

: 92264-98-7
N-(tert-butoxycarbonyl)-O-(dibenzylphosphono)-L-tyrosyl p-nitro-benzyl ester

Guidance literature:: With sodium hydride; 1) dioxan, 10-15 deg C, 30 min, 2) 1h, room temp.;
DOI:10.1016/S0040-4039(01)81243-0

Reference yield:

: 3978-80-1
Boc-Tyr-OH

: 92264-98-7
N-(tert-butoxycarbonyl)-O-(dibenzylphosphono)-L-tyrosyl p-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethyl acetate / 80 - 90 °C

2: triethylamine, CCl₄ / ethyl acetate

With tetrachloromethane; triethylamine; In ethyl acetate;
DOI:10.1021/ja00252a007

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 92264-98-7
N-(tert-butoxycarbonyl)-O-(dibenzylphosphono)-L-tyrosyl p-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethyl acetate / 80 - 90 °C

2: triethylamine, CCl₄ / ethyl acetate

With tetrachloromethane; triethylamine; In ethyl acetate;
DOI:10.1021/ja00252a007