(S)-2-[3-methyl-3H-thiazol-(2E)-ylideneamino]-4-tritylsulfanyl-butyric acid

Base Information

Chemical Name:(S)-2-[3-methyl-3H-thiazol-(2E)-ylideneamino]-4-tritylsulfanyl-butyric acid
CAS No.:1200836-56-1
Molecular Formula:C₂₇H₂₆N₂O₂S₂
Molecular Weight:474.648
Hs Code.:

Synonyms:(S)-2-[3-methyl-3H-thiazol-(2E)-ylideneamino]-4-tritylsulfanyl-butyric acid

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Chemical Property of (S)-2-[3-methyl-3H-thiazol-(2E)-ylideneamino]-4-tritylsulfanyl-butyric acid

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Technology Process of (S)-2-[3-methyl-3H-thiazol-(2E)-ylideneamino]-4-tritylsulfanyl-butyric acid

There total 5 articles about (S)-2-[3-methyl-3H-thiazol-(2E)-ylideneamino]-4-tritylsulfanyl-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1200836-52-7
(S)-2-(thiazol-2-ylamino)-4-tritylsulfanyl-butyric acid

: 74-88-4
methyl iodide

: 1200836-55-0
(S)-2-(methyl-thiazol-2-yl-amino)-4-tritylsulfanyl-butyric acid

: 1200836-56-1
(S)-2-[3-methyl-3H-thiazol-(2E)-ylideneamino]-4-tritylsulfanyl-butyric acid

Guidance literature:: (S)-2-(thiazol-2-ylamino)-4-tritylsulfanyl-butyric acid; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h;

methyl iodide; In tetrahydrofuran; mineral oil; at 20 ℃; for 24h;

With potassium hydrogensulfate; In tetrahydrofuran; water; mineral oil; pH=~ 3;

Reference yield:

: 76-84-6
triphenylmethyl alcohol

: 1200836-56-1
(S)-2-[3-methyl-3H-thiazol-(2E)-ylideneamino]-4-tritylsulfanyl-butyric acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonia; sodium / -78 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: potassium carbonate / copper(l) iodide; N,N`-dimethylethylenediamine / toluene / 24 h / 90 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

3.2: 24 h / 20 °C

3.3: pH ~ 3

With ammonia; sodium; sodium hydride; potassium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine; In tetrahydrofuran; toluene; mineral oil;

Reference yield:

: 69955-57-3
(2S)-2-amino-4-(tritylsulfanyl)butanoic acid

: 1200836-56-1
(S)-2-[3-methyl-3H-thiazol-(2E)-ylideneamino]-4-tritylsulfanyl-butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / copper(l) iodide; N,N`-dimethylethylenediamine / toluene / 24 h / 90 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

2.2: 24 h / 20 °C

2.3: pH ~ 3

With sodium hydride; potassium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine; In tetrahydrofuran; toluene; mineral oil;