(η5-C5H5)Fe(η2-Ph2PCH2CH2PPh2)F

Base Information

Chemical Name:(η5-C5H5)Fe(η2-Ph2PCH2CH2PPh2)F
CAS No.:207290-19-5
Molecular Formula:C₃₆H₃₉FFeP₂
Molecular Weight:608.499
Hs Code.:

Synonyms:(η5-C5H5)Fe(η2-Ph2PCH2CH2PPh2)F

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Chemical Property of (η5-C5H5)Fe(η2-Ph2PCH2CH2PPh2)F

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Technology Process of (η5-C5H5)Fe(η2-Ph2PCH2CH2PPh2)F

There total 2 articles about (η5-C5H5)Fe(η2-Ph2PCH2CH2PPh2)F which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 207290-22-0
[Cp*(1,2-bis(diphenylphosphanyl)ethane)FeF]PF₆

: 207290-19-5
(η5-C5H5)Fe(η2-Ph2PCH2CH2PPh2)F

Guidance literature:: With Cp₂Co; In tetrahydrofuran; under Ar atm. Cp2Co was added to cooled (-100°C) soln. Cp*Fe(dppe)FPF6 in THF and stirred overnight at room temp.;
DOI:10.1021/ja0106927

Reference yield: 86.0%

: 172987-51-8
[Cp*(1,2-bis(diphenylphosphanyl)ethane)Fe]PF₆

: 13400-13-0
cesium fluoride

: 207290-19-5
(η5-C5H5)Fe(η2-Ph2PCH2CH2PPh2)F

Guidance literature:: In tetrahydrofuran; under Ar atm. CsF was added to THF soln. Cp*Fe(dppe)PF6 at room temp. and stirred overnight; solvent was removed under vac., residue was extd. with Et2O and evapd. to dryness;
DOI:10.1021/ja0106927

Reference yield: 87.0%

: ferrocenium hexafluorophosphate

: 207290-19-5
(η5-C5H5)Fe(η2-Ph2PCH2CH2PPh2)F

: 207290-22-0
[Cp*(1,2-bis(diphenylphosphanyl)ethane)FeF]PF₆

Guidance literature:: In tetrahydrofuran; under Ar THF soln. Cp*Fe(dppe)F was treated with Cp2FePF6 and stirred for 15 min; solvent was removed under vac., residue was washed with Et2O; elem. anal.;
DOI:10.1021/ja0106927