5-((7-bromo-4-oxo-3,4-dihydrophthalazin-1-yl)methyl)-2-fluorobenzonitrile

Base Information

Chemical Name:5-((7-bromo-4-oxo-3,4-dihydrophthalazin-1-yl)methyl)-2-fluorobenzonitrile
CAS No.:1174044-55-3
Molecular Formula:C₁₆H₉BrFN₃O
Molecular Weight:358.169
Hs Code.:

Synonyms:5-((7-bromo-4-oxo-3,4-dihydrophthalazin-1-yl)methyl)-2-fluorobenzonitrile

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Chemical Property of 5-((7-bromo-4-oxo-3,4-dihydrophthalazin-1-yl)methyl)-2-fluorobenzonitrile

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Technology Process of 5-((7-bromo-4-oxo-3,4-dihydrophthalazin-1-yl)methyl)-2-fluorobenzonitrile

There total 1 articles about 5-((7-bromo-4-oxo-3,4-dihydrophthalazin-1-yl)methyl)-2-fluorobenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.4%

: 1174044-54-2
(6-bromo-3-oxo-1,3-dihydroisobenzofuran-1-yl)triphenylphosphonium bromide

: 218301-22-5
2-fluoro-5-formylbenzonitrile

: 1174044-55-3
5-((7-bromo-4-oxo-3,4-dihydrophthalazin-1-yl)methyl)-2-fluorobenzonitrile

Guidance literature:: (6-bromo-3-oxo-1,3-dihydroisobenzofuran-1-yl)triphenylphosphonium bromide; 2-fluoro-5-formylbenzonitrile; With triethylamine; In dichloromethane;

With hydrazine hydrate; In ethanol; water; N,N-dimethyl-formamide; Heating; Reflux;

Reference yield: 79.0%

: 1174044-55-3
5-((7-bromo-4-oxo-3,4-dihydrophthalazin-1-yl)methyl)-2-fluorobenzonitrile

: 1174044-56-4
5-((7-bromo-4-oxo-3,4-dihydrophthalazin-1-yl)methyl)-2-fluorobenzoic acid

Guidance literature:: 5-((7-bromo-4-oxo-3,4-dihydrophthalazin-1-yl)methyl)-2-fluorobenzonitrile; With water; potassium hydroxide; In ethanol; at 100 ℃; for 5h;

With hydrogenchloride; water; pH=1;