4,4'-bis(2,5-dibutoxy-4-(2,5-dimethoxy-4-dibutylaminostyryl)styryl)-2,2'-bipyridine

Base Information

Chemical Name:4,4'-bis(2,5-dibutoxy-4-(2,5-dimethoxy-4-dibutylaminostyryl)styryl)-2,2'-bipyridine
CAS No.:1350615-92-7
Molecular Formula:C₇₈H₁₀₆N₄O₈
Molecular Weight:1227.72
Hs Code.:

Synonyms:4,4'-bis(2,5-dibutoxy-4-(2,5-dimethoxy-4-dibutylaminostyryl)styryl)-2,2'-bipyridine

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Chemical Property of 4,4'-bis(2,5-dibutoxy-4-(2,5-dimethoxy-4-dibutylaminostyryl)styryl)-2,2'-bipyridine

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Technology Process of 4,4'-bis(2,5-dibutoxy-4-(2,5-dimethoxy-4-dibutylaminostyryl)styryl)-2,2'-bipyridine

There total 8 articles about 4,4'-bis(2,5-dibutoxy-4-(2,5-dimethoxy-4-dibutylaminostyryl)styryl)-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1350616-06-6
(E)-2,5-dibutoxy-4-(4-(dibutylamino)-2,5-dimethoxystyryl)benzaldehyde

: 176220-38-5
4,4'-bis(diethylphosphonomethyl)-2,2'-bipyridine

: 1350615-92-7
4,4'-bis(2,5-dibutoxy-4-(2,5-dimethoxy-4-dibutylaminostyryl)styryl)-2,2'-bipyridine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo202015m

Reference yield:

: 960081-01-0
diethyl (2,5-bisbutoxy-4-bromobenzyl)phosphonate

: 1350615-92-7
4,4'-bis(2,5-dibutoxy-4-(2,5-dimethoxy-4-dibutylaminostyryl)styryl)-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 1 h / -40 °C

2.2: 1 h / -40 °C

3.1: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

With n-butyllithium; potassium tert-butylate; In tetrahydrofuran; 1.1: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/jo202015m

Reference yield:

: 84311-83-1
1,4-dimethoxy-2-(N,N-dibutylamino)benzene

: 1350615-92-7
4,4'-bis(2,5-dibutoxy-4-(2,5-dimethoxy-4-dibutylaminostyryl)styryl)-2,2'-bipyridine

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / 4.25 h / 95 °C / Cooling with ice; Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran / 1 h / -40 °C

3.2: 1 h / -40 °C

4.1: potassium tert-butylate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

With n-butyllithium; potassium tert-butylate; trichlorophosphate; In tetrahydrofuran; 2.1: Horner-Wadsworth-Emmons olefination;
DOI:10.1021/jo202015m