2-(2-{2-[2-(3-{4-[2-(2,6-dimethyl-4-tritylphenoxy)ethoxy]phenyl}propoxy)ethoxy]ethoxy}ethoxy)ethanol

Base Information

Chemical Name:2-(2-{2-[2-(3-{4-[2-(2,6-dimethyl-4-tritylphenoxy)ethoxy]phenyl}propoxy)ethoxy]ethoxy}ethoxy)ethanol
CAS No.:881890-60-4
Molecular Formula:C₄₆H₅₄O₇
Molecular Weight:718.931
Hs Code.:

Synonyms:2-(2-{2-[2-(3-{4-[2-(2,6-dimethyl-4-tritylphenoxy)ethoxy]phenyl}propoxy)ethoxy]ethoxy}ethoxy)ethanol

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Chemical Property of 2-(2-{2-[2-(3-{4-[2-(2,6-dimethyl-4-tritylphenoxy)ethoxy]phenyl}propoxy)ethoxy]ethoxy}ethoxy)ethanol

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Technology Process of 2-(2-{2-[2-(3-{4-[2-(2,6-dimethyl-4-tritylphenoxy)ethoxy]phenyl}propoxy)ethoxy]ethoxy}ethoxy)ethanol

There total 7 articles about 2-(2-{2-[2-(3-{4-[2-(2,6-dimethyl-4-tritylphenoxy)ethoxy]phenyl}propoxy)ethoxy]ethoxy}ethoxy)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 881890-58-0
2-{2-[4-(3-bromopropyl)phenoxy]ethoxy}-1,3-dimethyl-5-tritylbenzene

: 112-60-7
Tetraethylene glycol

: 881890-60-4
2-(2-{2-[2-(3-{4-[2-(2,6-dimethyl-4-tritylphenoxy)ethoxy]phenyl}propoxy)ethoxy]ethoxy}ethoxy)ethanol

Guidance literature:: Tetraethylene glycol; With sodium ethanolate; In dimethyl sulfoxide; at 70 ℃; for 0.25h;

2-{2-[4-(3-bromopropyl)phenoxy]ethoxy}-1,3-dimethyl-5-tritylbenzene; In dimethyl sulfoxide; at 90 ℃; for 1.5h;
DOI:10.1002/ejoc.200500421

Reference yield:

: 881890-42-2
2,6-dimethyl-4-tritylphenol

: 881890-60-4
2-(2-{2-[2-(3-{4-[2-(2,6-dimethyl-4-tritylphenoxy)ethoxy]phenyl}propoxy)ethoxy]ethoxy}ethoxy)ethanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 86 percent / NaOEt / acetonitrile / 16 h / Heating

2.1: 99 percent / NaOEt / acetonitrile / 6 h / Heating

3.1: 87 percent / 2,6-di-tert-butyl-4-methylpyridine; PBr₃ / CH₂Cl₂ / 2 h / -30 °C

4.1: NaOEt / dimethylsulfoxide / 0.25 h / 70 °C

4.2: 68 percent / dimethylsulfoxide / 1.5 h / 90 °C

With 2,6-di-tert-butyl-4-methylpyridine; sodium ethanolate; phosphorus tribromide; In dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1002/ejoc.200500421

Reference yield:

: 881890-56-8
2-(2,6-dimethyl-4-tritylphenoxy)ethyl toluene-4-sulfonate

: 881890-60-4
2-(2-{2-[2-(3-{4-[2-(2,6-dimethyl-4-tritylphenoxy)ethoxy]phenyl}propoxy)ethoxy]ethoxy}ethoxy)ethanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 99 percent / NaOEt / acetonitrile / 6 h / Heating

2.1: 87 percent / 2,6-di-tert-butyl-4-methylpyridine; PBr₃ / CH₂Cl₂ / 2 h / -30 °C

3.1: NaOEt / dimethylsulfoxide / 0.25 h / 70 °C

3.2: 68 percent / dimethylsulfoxide / 1.5 h / 90 °C

With 2,6-di-tert-butyl-4-methylpyridine; sodium ethanolate; phosphorus tribromide; In dichloromethane; dimethyl sulfoxide; acetonitrile;
DOI:10.1002/ejoc.200500421