(R,S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2(1H)-sulfonamide

Base Information

Chemical Name:(R,S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2(1H)-sulfonamide
CAS No.:1161432-33-2
Molecular Formula:C₁₇H₂₀N₂O₄S
Molecular Weight:348.423
Hs Code.:

Synonyms:(R,S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2(1H)-sulfonamide

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Chemical Property of (R,S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2(1H)-sulfonamide

Chemical Property:

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Technology Process of (R,S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2(1H)-sulfonamide

There total 4 articles about (R,S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2(1H)-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 4118-36-9
6,7-dimethoxy-1-phenyl-1,2,3,4-tetrahydroisoquinoline

: 1161432-33-2
(R,S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2(1H)-sulfonamide

Guidance literature:: With SULFAMIDE; In 1,1-dimethoxyethane; at 90 ℃; for 0.666667h; under 10343.2 Torr; Microwave irradiation;
DOI:10.1016/j.bmc.2009.03.066

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 1161432-33-2
(R,S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2(1H)-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 0.08 h / 90 °C / 10351 Torr / Microwave irradiation

2: trifluoroacetic acid / 0.08 h / 90 °C / 10351 Torr / Microwave irradiation

3: 1,1-dimethoxyethane; SULFAMIDE / 0.33 h / 10351 Torr / Heating; Microwave irradiation

With 1,1-dimethoxyethane; SULFAMIDE; trifluoroacetic acid;
DOI:10.1002/cmdc.201500596

Reference yield:

: 10133-74-1
N-phenylmethylene-2-(3,4-dimethoxyphenyl)ethylamine

: 1161432-33-2
(R,S)-6,7-dimethoxy-1-phenyl-3,4-dihydroisoquinoline-2(1H)-sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 0.08 h / 90 °C / 10351 Torr / Microwave irradiation

2: 1,1-dimethoxyethane; SULFAMIDE / 0.33 h / 10351 Torr / Heating; Microwave irradiation

With 1,1-dimethoxyethane; SULFAMIDE; trifluoroacetic acid;
DOI:10.1002/cmdc.201500596