N,N'-bis(3-ethoxysalicylidene)-1-methylethylenediamine

Base Information

• Chemical Name: N,N'-bis(3-ethoxysalicylidene)-1-methylethylenediamine
• CAS No.: 1086091-22-6
• Molecular Formula: C₂₁H₂₆N₂O₄
• Molecular Weight: 370.448
• Mol file: 1086091-22-6.mol

Synonyms:N,N'-bis(3-ethoxysalicylidene)-1-methylethylenediamine

Chemical Property of N,N'-bis(3-ethoxysalicylidene)-1-methylethylenediamine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of N,N'-bis(3-ethoxysalicylidene)-1-methylethylenediamine

There total 1 articles about N,N'-bis(3-ethoxysalicylidene)-1-methylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.3%

3-ethoxysalicylaldehyde (492-88-6) + 1,2-diaminopropan (78-90-0,10424-38-1) → N,N'-bis(3-ethoxysalicylidene)-1-methylethylenediamine (1086091-22-6)

Guidance literature:

In ethanol; at 50 ℃; for 2h;

DOI:10.1071/CH11291

Reference yield: 63.5%

sodium azide + N,N'-bis(3-ethoxysalicylidene)-1-methylethylenediamine (1086091-22-6) + cadmium(II) acetate dihydrate (5743-04-4) → 4C21H24N2O4(2-)*8Cd(2+)*6N3(1-)*2C2H3O2(1-)

Guidance literature:

In methanol; water; acetonitrile; at 70 ℃; for 3h;

DOI:10.1016/j.molstruc.2018.11.010

Reference yield:

N,N'-bis(3-ethoxysalicylidene)-1-methylethylenediamine (1086091-22-6) → [(1,2-propanediyl)bis(iminomethylene)bis(6-ethoxyphenol)]

Guidance literature:

N,N'-bis(3-ethoxysalicylidene)-1-methylethylenediamine; With sodium tetrahydroborate; In methanol; at 0 ℃;

With acetic acid; In methanol;

DOI:10.1039/c9dt01818b

upstream raw materials:

3-ethoxysalicylaldehyde

1,2-diaminopropan