4'-Hydroxymethyl-3,4-dimethoxy-6-methyl-bicyclohexyl-3,6-diene-2,5-dione

Base Information

Chemical Name:4'-Hydroxymethyl-3,4-dimethoxy-6-methyl-bicyclohexyl-3,6-diene-2,5-dione
CAS No.:144851-04-7
Molecular Formula:C₁₆H₂₂O₅
Molecular Weight:294.348
Hs Code.:

Synonyms:4'-Hydroxymethyl-3,4-dimethoxy-6-methyl-bicyclohexyl-3,6-diene-2,5-dione

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Chemical Property of 4'-Hydroxymethyl-3,4-dimethoxy-6-methyl-bicyclohexyl-3,6-diene-2,5-dione

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Technology Process of 4'-Hydroxymethyl-3,4-dimethoxy-6-methyl-bicyclohexyl-3,6-diene-2,5-dione

There total 12 articles about 4'-Hydroxymethyl-3,4-dimethoxy-6-methyl-bicyclohexyl-3,6-diene-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(4-Hydroxymethyl-cyclohexyl)-5,6-dimethoxy-3-methyl-benzene-1,4-diol

: 144851-04-7
4'-Hydroxymethyl-3,4-dimethoxy-6-methyl-bicyclohexyl-3,6-diene-2,5-dione

Guidance literature:: With iron(III) chloride; In tetrahydrofuran; hydrogenchloride; diethyl ether; for 1h; Yield given; Heating;
DOI:10.1021/jo970752k

Reference yield:

: 605-94-7
2,3-Dimethoxy-5-methyl-1,4-benzoquinone

: 144851-04-7
4'-Hydroxymethyl-3,4-dimethoxy-6-methyl-bicyclohexyl-3,6-diene-2,5-dione

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium peroxodisulfate, AgNO₃ / H₂O; CH₂Cl₂ / Heating

2: Na₂S₂O₄ / H₂O; CH₂Cl₂

3: LiBH₄ / tetrahydrofuran / 20 h / Heating

4: FeCl₃ / tetrahydrofuran; aq. HCl; diethyl ether / 1 h / Heating

With ammonium persulfate; lithium borohydride; sodium dithionite; iron(III) chloride; silver nitrate; In tetrahydrofuran; hydrogenchloride; diethyl ether; dichloromethane; water;
DOI:10.1021/jo970752k

Reference yield:

: 32529-79-6
4-(methoxycarbonyl)cyclohexanecarboxylic acid

: 144851-04-7
4'-Hydroxymethyl-3,4-dimethoxy-6-methyl-bicyclohexyl-3,6-diene-2,5-dione

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium peroxodisulfate, AgNO₃ / H₂O; CH₂Cl₂ / Heating

2: Na₂S₂O₄ / H₂O; CH₂Cl₂

3: LiBH₄ / tetrahydrofuran / 20 h / Heating

4: FeCl₃ / tetrahydrofuran; aq. HCl; diethyl ether / 1 h / Heating

With ammonium persulfate; lithium borohydride; sodium dithionite; iron(III) chloride; silver nitrate; In tetrahydrofuran; hydrogenchloride; diethyl ether; dichloromethane; water;
DOI:10.1021/jo970752k