2-(1-(2-nitrophenylsulfonamido)nonan-2-ylidene)propane-1,3-diyl diacetate

Base Information

• Chemical Name: 2-(1-(2-nitrophenylsulfonamido)nonan-2-ylidene)propane-1,3-diyl diacetate
• CAS No.: 1442642-88-7
• Molecular Formula: C₂₂H₃₂N₂O₈S
• Molecular Weight: 484.571

Synonyms:2-(1-(2-nitrophenylsulfonamido)nonan-2-ylidene)propane-1,3-diyl diacetate

Chemical Property of 2-(1-(2-nitrophenylsulfonamido)nonan-2-ylidene)propane-1,3-diyl diacetate

Chemical Property:

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Technology Process of 2-(1-(2-nitrophenylsulfonamido)nonan-2-ylidene)propane-1,3-diyl diacetate

There total 9 articles about 2-(1-(2-nitrophenylsulfonamido)nonan-2-ylidene)propane-1,3-diyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-2-nitrobenzenesulfonamide (1442642-82-1) + (Z)-2-(1-hydroxy-3-methoxypropan-2-ylidene)nonyl-2-nitrobenzenesulfonamide (1442642-38-7) + acetic anhydride (108-24-7) → (E)-2-(hydroxymethyl)-3-((2-nitrophenylsulfonamido)methyl)dec-2-enyl acetate (1442642-69-4) + (Z)-2-(hydroxymethyl)-3-((2-nitrophenylsulfonamido)methyl)dec-2-enyl acetate (1442642-70-7) + 2-(1-(2-nitrophenylsulfonamido)nonan-2-ylidene)propane-1,3-diyl diacetate (1442642-88-7) + (E)-2-(methoxymethyl)-3-((2-nitrobenzenesulfonamido)methyl)dec-2-enyl acetate (1442642-36-5)

Guidance literature:

N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-2-nitrobenzenesulfonamide; (Z)-2-(1-hydroxy-3-methoxypropan-2-ylidene)nonyl-2-nitrobenzenesulfonamide; With 2,4,6-trimethyl-pyridine; (2S,5S)-2,5-bis[[(2S)-3-(2-naphthylmethyl)-1-(octyloxy)-1-oxopropan-2-ylamino]carbonyl]-1-(pyridin-4-yl)pyrrolidine; In chloroform; at 20 ℃; for 0.25h;

acetic anhydride; In chloroform; at -60 ℃; for 24h; diastereoselective reaction;

DOI:10.1002/adsc.201200242

Reference yield: 92.0%

N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-2-nitrobenzenesulfonamide (1442642-82-1) + (E)-2-(1-hydroxy-3-methoxypropan-2-ylidene)nonyl-2-nitrobenzenesulfonamide (1442642-39-8) + acetic anhydride (108-24-7) → (E)-2-(hydroxymethyl)-3-((2-nitrophenylsulfonamido)methyl)dec-2-enyl acetate (1442642-69-4) + (Z)-2-(hydroxymethyl)-3-((2-nitrophenylsulfonamido)methyl)dec-2-enyl acetate (1442642-70-7) + 2-(1-(2-nitrophenylsulfonamido)nonan-2-ylidene)propane-1,3-diyl diacetate (1442642-88-7) + (Z)-2-(methoxymethyl)-3-((2-nitrobenzenesulfonamido)methyl)dec-2-enyl acetate (1442642-37-6)

Guidance literature:

N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-2-nitrobenzenesulfonamide; (E)-2-(1-hydroxy-3-methoxypropan-2-ylidene)nonyl-2-nitrobenzenesulfonamide; With 2,4,6-trimethyl-pyridine; (2S,5S)-2,5-bis[[(2S)-3-(2-naphthylmethyl)-1-(octyloxy)-1-oxopropan-2-ylamino]carbonyl]-1-(pyridin-4-yl)pyrrolidine; In chloroform; at 20 ℃; for 0.25h;

acetic anhydride; In chloroform; at -60 ℃; for 24h; diastereoselective reaction;

DOI:10.1002/adsc.201200242

Reference yield: 91.0%

N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-2-nitrobenzenesulfonamide (1442642-82-1) + N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide (1442642-89-8) + acetic anhydride (108-24-7) → (E)-2-(hydroxymethyl)-3-((2-nitrophenylsulfonamido)methyl)dec-2-enyl acetate (1442642-69-4) + (Z)-2-(hydroxymethyl)-3-((2-nitrophenylsulfonamido)methyl)dec-2-enyl acetate (1442642-70-7) + (E)-2-(hydroxymethyl)-3-((N-methyl-2-nitrobenzenesulfonamido)methyl)dec-2-enyl acetate (1442642-35-4) + (Z)-2-(hydroxymethyl)-3-((N-methyl-2-nitrobenzenesulfonamido)methyl)dec-2-enyl acetate (1442642-87-6) + 2-(1-(2-nitrophenylsulfonamido)nonan-2-ylidene)propane-1,3-diyl diacetate (1442642-88-7) + 2-(1-(N-methyl-2-nitrophenylsulfonamido)nonan-2-ylidene)propane-1,3-diyl diacetate (1442642-33-2)

Guidance literature:

N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-2-nitrobenzenesulfonamide; N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide; With 2,4,6-trimethyl-pyridine; (2S,5S)-2,5-bis[[(2S)-3-(2-naphthylmethyl)-1-(octyloxy)-1-oxopropan-2-ylamino]carbonyl]-1-(pyridin-4-yl)pyrrolidine; In chloroform; at 20 ℃; for 0.25h;

acetic anhydride; In chloroform; at -60 ℃; for 24h; diastereoselective reaction;

DOI:10.1002/adsc.201200242

upstream raw materials:

Ethyl 2-(diethoxyphosphinyl)-nonanoate

N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-2-nitrobenzenesulfonamide

N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide

acetic anhydride

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