1-benzyl-2-butyl-1H-imidazo[4,5-c]pyridin-4-amine

Base Information

Chemical Name:1-benzyl-2-butyl-1H-imidazo[4,5-c]pyridin-4-amine
CAS No.:1457966-67-4
Molecular Formula:C₁₇H₂₀N₄
Molecular Weight:280.373
Hs Code.:

Synonyms:1-benzyl-2-butyl-1H-imidazo[4,5-c]pyridin-4-amine

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Chemical Property of 1-benzyl-2-butyl-1H-imidazo[4,5-c]pyridin-4-amine

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Technology Process of 1-benzyl-2-butyl-1H-imidazo[4,5-c]pyridin-4-amine

There total 7 articles about 1-benzyl-2-butyl-1H-imidazo[4,5-c]pyridin-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1457966-66-3
1-benzyl-2-butyl-1H-imidazo[4,5-c]pyridine 5-oxide

: 1457966-67-4
1-benzyl-2-butyl-1H-imidazo[4,5-c]pyridin-4-amine

Guidance literature:: 1-benzyl-2-butyl-1H-imidazo[4,5-c]pyridine 5-oxide; With benzoyl isocyanate; In dichloromethane; at 45 ℃; for 2h;

With sodium methylate; In methanol; at 80 ℃; for 1h;
DOI:10.1039/c3ob40816g

Reference yield:

: 13091-23-1
4-chloro-3-nitropyridine

: 1457966-67-4
1-benzyl-2-butyl-1H-imidazo[4,5-c]pyridin-4-amine

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 18 h / Reflux

2.1: zinc; ammonium formate / methanol / 0.17 h / 20 °C

3.1: triethylamine / tetrahydrofuran / 2 h / Reflux

4.1: sodium hydroxide / ethanol; water / 4 h / Reflux

5.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 1 h / 45 - 50 °C

6.1: benzoyl isocyanate / dichloromethane / 2 h / 45 °C

6.2: 1 h / 80 °C

With ammonium formate; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; benzoyl isocyanate; zinc; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; water;
DOI:10.1039/c3ob40816g

Reference yield:

: 100-46-9
benzylamine

: 1457966-67-4
1-benzyl-2-butyl-1H-imidazo[4,5-c]pyridin-4-amine

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / dichloromethane / 18 h / Reflux

2.1: zinc; ammonium formate / methanol / 0.17 h / 20 °C

3.1: triethylamine / tetrahydrofuran / 2 h / Reflux

4.1: sodium hydroxide / ethanol; water / 4 h / Reflux

5.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 1 h / 45 - 50 °C

6.1: benzoyl isocyanate / dichloromethane / 2 h / 45 °C

6.2: 1 h / 80 °C

With ammonium formate; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; benzoyl isocyanate; zinc; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; water;
DOI:10.1039/c3ob40816g