(2R,3R)-1-phenyl-r-1,c-2,t-3-trideuteriocyclopropane

Base Information

Chemical Name:(2R,3R)-1-phenyl-r-1,c-2,t-3-trideuteriocyclopropane
CAS No.:88546-86-5
Molecular Formula:C₉H₁₀
Molecular Weight:121.155
Hs Code.:

Synonyms:(2R,3R)-1-phenyl-r-1,c-2,t-3-trideuteriocyclopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-1-phenyl-r-1,c-2,t-3-trideuteriocyclopropane

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Technology Process of (2R,3R)-1-phenyl-r-1,c-2,t-3-trideuteriocyclopropane

There total 6 articles about (2R,3R)-1-phenyl-r-1,c-2,t-3-trideuteriocyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52751-11-8
cis<α,β-2H2>styrene

: 88546-86-5
(2R,3R)-1-phenyl-r-1,c-2,t-3-trideuteriocyclopropane

Guidance literature:: Multi-step reaction with 5 steps

1: 63 percent / chiral copper(II) catalyst / cyclohexane / 67 °C

2: 96 percent / 25 percent aq. NaOH / methanol / 12.5 h / Heating

3: 96 percent / LiAlH₄ / tetrahydrofuran

4: 2.5 percent / pyridinium chlorochromate

5: 63 percent / chlorotris(triphenylphosphine)rhodium(I) / benzene / 17 h / Heating

With sodium hydroxide; Wilkinson's catalyst; lithium aluminium tetrahydride; pyridinium chlorochromate; chiral copper(II) catalyst; In tetrahydrofuran; methanol; cyclohexane; benzene;
DOI:10.1021/ja00317a038

Reference yield:

: 80594-26-9
(+)-(1S,2S,3S)-t-2-phenyl-1,2,c-3-trideuteriocyclopropylmethanol

: 88546-86-5
(2R,3R)-1-phenyl-r-1,c-2,t-3-trideuteriocyclopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 2.5 percent / pyridinium chlorochromate

2: 63 percent / chlorotris(triphenylphosphine)rhodium(I) / benzene / 17 h / Heating

With Wilkinson's catalyst; pyridinium chlorochromate; In benzene;
DOI:10.1021/ja00317a038

Reference yield:

: 80594-21-4
(+)-(1S,2S,3S)-t-2-phenyl-1,2,c-3-trideuteriocyclopropanecarboxylic acid

: 88546-86-5
(2R,3R)-1-phenyl-r-1,c-2,t-3-trideuteriocyclopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / LiAlH₄ / tetrahydrofuran

2: 2.5 percent / pyridinium chlorochromate

3: 63 percent / chlorotris(triphenylphosphine)rhodium(I) / benzene / 17 h / Heating

With Wilkinson's catalyst; lithium aluminium tetrahydride; pyridinium chlorochromate; In tetrahydrofuran; benzene;
DOI:10.1021/ja00317a038