allyl (3aβ,12β,12aβ,12bβ)-1,2,3,3a,4,5,11,12,12a,12b-decahydro-9-(benzyloxy)-3aβ-ethyl-5-oxoisoquino<2,1,8-lma>carbazole-12-carboxylate

Base Information

Chemical Name:allyl (3aβ,12β,12aβ,12bβ)-1,2,3,3a,4,5,11,12,12a,12b-decahydro-9-(benzyloxy)-3aβ-ethyl-5-oxoisoquino<2,1,8-lma>carbazole-12-carboxylate
CAS No.:103558-71-0
Molecular Formula:C₃₁H₃₃NO₄
Molecular Weight:483.607
Hs Code.:

Synonyms:allyl (3aβ,12β,12aβ,12bβ)-1,2,3,3a,4,5,11,12,12a,12b-decahydro-9-(benzyloxy)-3aβ-ethyl-5-oxoisoquino<2,1,8-lma>carbazole-12-carboxylate

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Chemical Property of allyl (3aβ,12β,12aβ,12bβ)-1,2,3,3a,4,5,11,12,12a,12b-decahydro-9-(benzyloxy)-3aβ-ethyl-5-oxoisoquino<2,1,8-lma>carbazole-12-carboxylate

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Technology Process of allyl (3aβ,12β,12aβ,12bβ)-1,2,3,3a,4,5,11,12,12a,12b-decahydro-9-(benzyloxy)-3aβ-ethyl-5-oxoisoquino<2,1,8-lma>carbazole-12-carboxylate

There total 4 articles about allyl (3aβ,12β,12aβ,12bβ)-1,2,3,3a,4,5,11,12,12a,12b-decahydro-9-(benzyloxy)-3aβ-ethyl-5-oxoisoquino<2,1,8-lma>carbazole-12-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103581-94-8
methyl (E)-3-<5-(benzyloxy)-1H-indol-3-yl>-2-propenoate

: 103558-71-0
allyl (3aβ,12β,12aβ,12bβ)-1,2,3,3a,4,5,11,12,12a,12b-decahydro-9-(benzyloxy)-3aβ-ethyl-5-oxoisoquino<2,1,8-lma>carbazole-12-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 75.1 percent / toluene / 20 h / Heating

2: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, 0.5 h

3: 2.) 15percent ethanol. HCl / 1.) mesitylene, reflux, 12 h, 2.) mesitylene, reflux, 0.5 h

With hydrogenchloride; sodium hydride; In toluene;
DOI:10.1021/jm00083a004

Reference yield:

: 103580-92-3
allyl (E)-3-<5-(benzyloxy)-1-<2-(1-ethyl-2-cyclohexen-1-yl)acetyl>-1H-indol-3-yl>-2-propenoate

: 103558-71-0
allyl (3aβ,12β,12aβ,12bβ)-1,2,3,3a,4,5,11,12,12a,12b-decahydro-9-(benzyloxy)-3aβ-ethyl-5-oxoisoquino<2,1,8-lma>carbazole-12-carboxylate

Guidance literature:: With hydrogenchloride; Yield given. Multistep reaction; 1.) mesitylene, reflux, 12 h, 2.) mesitylene, reflux, 0.5 h;
DOI:10.1021/jm00083a004

Reference yield:

: 103580-91-2
allyl (E)-3-<5-(benzyloxy)-1H-indol-3-yl>-2-propenoate

: 103558-71-0
allyl (3aβ,12β,12aβ,12bβ)-1,2,3,3a,4,5,11,12,12a,12b-decahydro-9-(benzyloxy)-3aβ-ethyl-5-oxoisoquino<2,1,8-lma>carbazole-12-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, 0.5 h

2: 2.) 15percent ethanol. HCl / 1.) mesitylene, reflux, 12 h, 2.) mesitylene, reflux, 0.5 h

With hydrogenchloride; sodium hydride;
DOI:10.1021/jm00083a004