4-benzyloxy-2-benzyloxycarbonylmethoxybenzaldehyde

Base Information

Chemical Name:4-benzyloxy-2-benzyloxycarbonylmethoxybenzaldehyde
CAS No.:910225-67-1
Molecular Formula:C₂₃H₂₀O₅
Molecular Weight:376.409
Hs Code.:

Synonyms:4-benzyloxy-2-benzyloxycarbonylmethoxybenzaldehyde

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Chemical Property of 4-benzyloxy-2-benzyloxycarbonylmethoxybenzaldehyde

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Technology Process of 4-benzyloxy-2-benzyloxycarbonylmethoxybenzaldehyde

There total 1 articles about 4-benzyloxy-2-benzyloxycarbonylmethoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 5437-45-6
Benzyl bromoacetate

: 52085-14-0
4-benzoxy-salicylaldehyde

: 910225-67-1
4-benzyloxy-2-benzyloxycarbonylmethoxybenzaldehyde

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ja061972v

Reference yield:

: 910225-67-1
4-benzyloxy-2-benzyloxycarbonylmethoxybenzaldehyde

: 26187-28-0
2,4-dimethyl-1H-pyrrole-3-carbonitrile

: 910225-68-2
C₃₇H₃₂N₄O₄

Guidance literature:: 4-benzyloxy-2-benzyloxycarbonylmethoxybenzaldehyde; 2,4-dimethyl-1H-pyrrole-3-carbonitrile; With trifluoroacetic acid; In dichloromethane; at 20 ℃;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 910225-67-1
4-benzyloxy-2-benzyloxycarbonylmethoxybenzaldehyde

: C₂₃H₁₉BF₂N₄O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / CH₂Cl₂ / 20 °C

1.2: 2,3-dichloro-5,6-dicyano-p-benzoquinone / CH₂Cl₂

2.1: 245 mg / diisopropylethylamine; BF₃*OEt₂ / toluene / 20 °C

3.1: 59 percent / H₂ / Pd/C / CHCl₃; ethanol

With boron trifluoride diethyl etherate; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In ethanol; dichloromethane; chloroform; toluene;
DOI:10.1021/ja061972v