4-amino-N-[1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichlorobenzenesulphonamide

Base Information

• Chemical Name: 4-amino-N-[1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichlorobenzenesulphonamide
• CAS No.: 152134-35-5
• Molecular Formula: C₂₂H₂₅Cl₂N₅O₃S
• Molecular Weight: 510.444

Synonyms:4-amino-N-[1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichlorobenzenesulphonamide

Chemical Property of 4-amino-N-[1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichlorobenzenesulphonamide

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Technology Process of 4-amino-N-[1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichlorobenzenesulphonamide

There total 1 articles about 4-amino-N-[1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichlorobenzenesulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Amino-N-[1-((4-amino-3-nitro-phenyl)-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichlorobenzenesulphonamide (152134-99-1) → 4-amino-N-[1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichlorobenzenesulphonamide (152134-35-5)

Guidance literature:

palladium/charcoal; In formic acid; water;

Reference yield: 25.0%

cis,trans-2,5-dimethoxytetrahydrofuran (696-59-3) + 4-amino-N-[1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichlorobenzenesulphonamide (152134-35-5) → N-[1-(1H-Benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichloro-4-pyrrolylbenzenesulphonamide

Guidance literature:

In methanol; acetic acid;

Reference yield: 18.0%

C24 H29 Cl2 N5 O3 S + 4-amino-N-[1-(1H-benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichlorobenzenesulphonamide (152134-35-5) → N-[1-(1H-Benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichloro-4-dimethylamino-benzenesulphonamide (152134-41-3)

Guidance literature:

With paraformaldehyde;

upstream raw materials:

4-Amino-N-[1-((4-amino-3-nitro-phenyl)-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichlorobenzenesulphonamide

Downstream raw materials:

N-[1-(1H-benzimidazol-5-yl-methyl)-2-(4-ethylpiperidin-1-yl)-2-oxo-ethyl]-3,5-dichloro-4-ethylamino-benzenesulphonamide

N-[1-(1H-Benzimidazol-5-yl-methyl)-2-(4-methyl-piperidin-1-yl)-2-oxo-ethyl]-3,5-dichloro-4-dimethylamino-benzenesulphonamide

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