{1,2-bis(diphenylphosphino)ethane-P,P'}tris(phenyl isocyanide)iron⁽⁰⁾

Base Information

Chemical Name:{1,2-bis(diphenylphosphino)ethane-P,P'}tris(phenyl isocyanide)iron⁽⁰⁾
CAS No.:121241-52-9
Molecular Formula:C₄₇H₃₉FeN₃P₂
Molecular Weight:763.641
Hs Code.:

{1,2-bis(diphenylphosphino)ethane-P,P'}tris(phenyl isocyanide)iron<sup>(0)</sup>

Synonyms:{1,2-bis(diphenylphosphino)ethane-P,P'}tris(phenyl isocyanide)iron⁽⁰⁾

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Chemical Property of {1,2-bis(diphenylphosphino)ethane-P,P'}tris(phenyl isocyanide)iron⁽⁰⁾

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Technology Process of {1,2-bis(diphenylphosphino)ethane-P,P'}tris(phenyl isocyanide)iron⁽⁰⁾

There total 1 articles about {1,2-bis(diphenylphosphino)ethane-P,P'}tris(phenyl isocyanide)iron⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95402-13-4
mer-{FeI(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}I

: 121241-52-9
{1,2-bis(diphenylphosphino)ethane-P,P'}tris(phenyl isocyanide)iron⁽⁰⁾

Guidance literature:: With Na#Hg; In tetrahydrofuran; dry oxygen-free argon atmosphere; addn. of excess of sodium amalgam to a stirred suspension of mer-{FeI(dppe)(CNPh)3}I in THF, stirred for 1 h, red soln. was filtered, solvent was removed in vacuo, residue extracted with toluene, filtration; no isolation;

Reference yield: 74.0%

: 121241-52-9
{1,2-bis(diphenylphosphino)ethane-P,P'}tris(phenyl isocyanide)iron⁽⁰⁾

: 74-88-4
methyl iodide

: {FeI(1,2-bis(diphenylphosphino)ethane-PP')(1,2-di(phenylimino)propyl-C₁N₂)(phenyl isocyanide)}

Guidance literature:: In toluene; dry oxygen-free argon atmosphere; freshly distilled CH3I was added to a soln. of {Fe(dppe)(CNPh)3}, darkening in the red color of the soln., mixture was stirred for 30 min, solvent was removed in vacuo, addn. of diethyl ether, cooling; elemental analysis;

Reference yield: 70.0%

: ammonium hexafluorophosphate

: 121241-52-9
{1,2-bis(diphenylphosphino)ethane-P,P'}tris(phenyl isocyanide)iron⁽⁰⁾

: 121241-56-3,121313-40-4
mer-{FeH(1,2-bis(diphenylphosphino)ethane)(phenyl isocyanide)3}PF₆

Guidance literature:: In toluene; dry oxygen-free argon atmosphere; to a soln. of {Fe(dppe)(CNPh)3} in toluene was added NH4PF6 in deaerated distilled water, stirred for 2 h, yellow ppt. was formed; filtration, washed with three successive portions of water, dried in vacuo; elemental analysis;