2-deoxy-2-[(2,4-dinitrophenyl)amino]hexitol

Base Information

• Chemical Name: 2-deoxy-2-[(2,4-dinitrophenyl)amino]hexitol
• CAS No.: 14278-76-3
• Molecular Formula: C₁₂H₁₇N₃O₉
• Molecular Weight: 347.282

Synonyms:Glucitol,2-deoxy-2-(2,4-dinitroanilino)-, D- (8CI);2-Deoxy-2-(2,4-dinitroanilino)-D-glucitol; N-(2,4-Dinitrophenyl)-2-amino-2-deoxy-D-glucitol;NSC 108116

Chemical Property of 2-deoxy-2-[(2,4-dinitrophenyl)amino]hexitol

Chemical Property:

• Vapor Pressure: 8.51E-24mmHg at 25°C
• Boiling Point: 752.6°Cat760mmHg
• Flash Point: 408.9°C
• Density: 1.701g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-deoxy-2-[(2,4-dinitrophenyl)amino]hexitol

There total 4 articles about 2-deoxy-2-[(2,4-dinitrophenyl)amino]hexitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-galactosamine (1948-54-5,2494-50-0,2636-92-2,3416-24-8,6915-39-5,7535-00-4,14307-02-9,14307-08-5,14307-09-6,14307-12-1,14307-14-3,14635-95-1,26315-48-0,27799-64-0,27799-65-1,69839-78-7,72904-60-0) → 2-(2,4-dinitro-anilino)-2-deoxy-D-galactitol (14278-76-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium borate; water

With sodium borate; water;

DOI:10.1021/ja01648a038

Reference yield:

2-amino-2-deoxy-D-glucitol hydrochloride (16981-00-3,58691-27-3) + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → 2-(2,4-dinitro-anilino)-2-deoxy-D-glucitol (14278-76-3)

Guidance literature:

With sodium hydrogencarbonate; In ethanol;

DOI:10.1016/S0008-6215(00)82050-9

Reference yield:

2-amino-2-deoxy-D-galacticol (20706-37-0,2351-14-6) + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → 2-(2,4-dinitro-anilino)-2-deoxy-D-galactitol (14278-76-3)

Guidance literature:

DOI:10.1021/ja01648a038

upstream raw materials:

2-amino-2-deoxy-D-glucitol

2,4-Dinitrofluorobenzene

2-amino-2-deoxy-D-glucitol hydrochloride

2-amino-2-deoxy-D-galacticol

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