{3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetic acid

Base Information

Chemical Name:{3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetic acid
CAS No.:1285513-74-7
Molecular Formula:C₂₂H₁₈ClNO₄
Molecular Weight:395.842
Hs Code.:

Synonyms:{3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetic acid

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Chemical Property of {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetic acid

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Technology Process of {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetic acid

There total 4 articles about {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1285516-40-6
methyl {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetate

: 1285513-74-7
{3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetic acid

Guidance literature:: With hydrogenchloride; water; acetic acid; at 90 ℃; for 4h;

Reference yield:

: 14338-36-4
3-amino phenylacetic acid

: 1285513-74-7
{3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / Reflux

1.2: pH 10

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.67 h / 60 °C / microwave irradiation

2.2: 0.33 h / 60 °C / microwave irradiation

3.1: hydrogenchloride; water; acetic acid / 4 h / 90 °C

With hydrogenchloride; sulfuric acid; water; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;

Reference yield:

: 321-14-2
5-chloro-2-hydroxybenzoic acid

: 1285513-74-7
{3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 20 - 60 °C

2.1: sodium hydroxide / ethanol / 2 h / Reflux

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.67 h / 60 °C / microwave irradiation

3.2: 0.33 h / 60 °C / microwave irradiation

4.1: hydrogenchloride; water; acetic acid / 4 h / 90 °C

With hydrogenchloride; water; potassium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;