methyl {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetate

Base Information

Chemical Name:methyl {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetate
CAS No.:1285516-40-6
Molecular Formula:C₂₃H₂₀ClNO₄
Molecular Weight:409.869
Hs Code.:

Synonyms:methyl {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetate

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Chemical Property of methyl {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetate

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Technology Process of methyl {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetate

There total 4 articles about methyl {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52803-75-5
2-(benzyloxy)-5-chlorobenzoic acid

: 52913-11-8
(3-amino-phenyl)-acetic acid methyl ester

: 1285516-40-6
methyl {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetate

Guidance literature:: 2-(benzyloxy)-5-chlorobenzoic acid; (3-amino-phenyl)-acetic acid methyl ester; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 60 ℃; for 0.666667h; microwave irradiation;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 60 ℃; for 0.333333h; microwave irradiation;

Reference yield:

: 14338-36-4
3-amino phenylacetic acid

: 1285516-40-6
methyl {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / Reflux

1.2: pH 10

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.67 h / 60 °C / microwave irradiation

2.2: 0.33 h / 60 °C / microwave irradiation

With sulfuric acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;

Reference yield:

: 321-14-2
5-chloro-2-hydroxybenzoic acid

: 1285516-40-6
methyl {3-[({5-chloro-2-[(phenylmethyl)oxy]phenyl}carbonyl)amino]phenyl}acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 20 - 60 °C

2.1: sodium hydroxide / ethanol / 2 h / Reflux

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.67 h / 60 °C / microwave irradiation

3.2: 0.33 h / 60 °C / microwave irradiation

With potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;