(5S,8S)-S-phenyl 8-benzyl-5-methyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triaza-dodecane-12-thioate

Base Information

Chemical Name:(5S,8S)-S-phenyl 8-benzyl-5-methyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triaza-dodecane-12-thioate
CAS No.:1384584-05-7
Molecular Formula:C₂₈H₂₉N₃O₅S
Molecular Weight:519.621
Hs Code.:

Synonyms:(5S,8S)-S-phenyl 8-benzyl-5-methyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triaza-dodecane-12-thioate

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Chemical Property of (5S,8S)-S-phenyl 8-benzyl-5-methyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triaza-dodecane-12-thioate

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Technology Process of (5S,8S)-S-phenyl 8-benzyl-5-methyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triaza-dodecane-12-thioate

There total 2 articles about (5S,8S)-S-phenyl 8-benzyl-5-methyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triaza-dodecane-12-thioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1342794-05-1
benzyl ((S)-1-(((S)-1-((2-(1H-benzo[d][1,2,3]triazol-1-yl)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

: 108-98-5
thiophenol

: 1384584-05-7
(5S,8S)-S-phenyl 8-benzyl-5-methyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triaza-dodecane-12-thioate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃;
DOI:10.1111/j.1747-0285.2012.01364.x

Reference yield:

: 16814-50-9,116460-40-3
(5S,8S)-8-benzyl-5-methyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triazadodecan-12-oic acid

: 1384584-05-7
(5S,8S)-S-phenyl 8-benzyl-5-methyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triaza-dodecane-12-thioate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / -45 °C

2: triethylamine / tetrahydrofuran / 20 °C

With thionyl chloride; triethylamine; In tetrahydrofuran;
DOI:10.1111/j.1747-0285.2012.01364.x