benzyl ((S)-1-(((S)-1-((2-(1H-benzo[d][1,2,3]triazol-1-yl)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

Base Information

• Chemical Name: benzyl ((S)-1-(((S)-1-((2-(1H-benzo[d][1,2,3]triazol-1-yl)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate
• CAS No.: 1342794-05-1
• Molecular Formula: C₂₈H₂₈N₆O₅
• Molecular Weight: 528.568

Synonyms:benzyl ((S)-1-(((S)-1-((2-(1H-benzo[d][1,2,3]triazol-1-yl)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

Chemical Property of benzyl ((S)-1-(((S)-1-((2-(1H-benzo[d][1,2,3]triazol-1-yl)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

Chemical Property:

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Technology Process of benzyl ((S)-1-(((S)-1-((2-(1H-benzo[d][1,2,3]triazol-1-yl)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

There total 1 articles about benzyl ((S)-1-(((S)-1-((2-(1H-benzo[d][1,2,3]triazol-1-yl)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1,2,3-Benzotriazole (95-14-7,27556-51-0) + (5S,8S)-8-benzyl-5-methyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triazadodecan-12-oic acid (16814-50-9,116460-40-3) → benzyl ((S)-1-(((S)-1-((2-(1H-benzo[d][1,2,3]triazol-1-yl)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate (1342794-05-1)

Guidance literature:

With thionyl chloride; at -45 ℃;

DOI:10.1111/j.1747-0285.2012.01364.x

Reference yield: 86.0%

L-alanin (56-41-7,25191-17-7,18875-37-1) + benzyl ((S)-1-(((S)-1-((2-(1H-benzo[d][1,2,3]triazol-1-yl)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate (1342794-05-1) → (5S,8S,14S)-8-benzyl-5,14-dimethyl-3,6,9,12-tetraoxo-1-phenyl-2-oxa-4,7,10,13-tetraazapentadecan-15-oic acid (50300-83-9)

Guidance literature:

With triethylamine; In water; acetonitrile; at 0 ℃;

DOI:10.1055/s-0030-1260159

Reference yield: 83.0%

benzyl ((S)-1-(((S)-1-((2-(1H-benzo[d][1,2,3]triazol-1-yl)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate (1342794-05-1) + Methyl thioglycolate (2365-48-2) → (5S,8S)-methyl 8-benzyl-5-methyl-3,6,9,12-tetraoxo-1-phenyl-2-oxa-13-thia-4,7,10-triazapentadecan-15-oate (1384584-06-8)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 ℃;

DOI:10.1111/j.1747-0285.2012.01364.x

upstream raw materials:

1,2,3-Benzotriazole

(5S,8S)-8-benzyl-5-methyl-3,6,9-trioxo-1-phenyl-2-oxa-4,7,10-triazadodecan-12-oic acid

Downstream raw materials:

benzyl ((S)-1-(((S)-1-((2-(((S)-1-(1H-benzo[d][1,2,3]triazol-1-yl)-1-oxopropan-2-yl)amino)-2-oxoethyl)amino)-1-oxo-3-phenylpropan-2-yl)amino)-1-oxopropan-2-yl)carbamate

Cbz-L-Ala-L-Phe-Gly-L-Ala-L-Phe-OH

Cbz-L-Ala-L-Phe-Gly-L-Ala-Gly-L-Leu-OH

Cbz-L-Ala-L-Phe-L-Gly-L-Ala-L-Phe-Bt

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