hydrazon obtained by condensation of 2-pyridylhydrazine with p-methoxyacetophenone

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Chemical Name:hydrazon obtained by condensation of 2-pyridylhydrazine with p-methoxyacetophenone
CAS No.:82664-05-9
Molecular Formula:C₁₄H₁₅N₃O
Molecular Weight:241.293
Hs Code.:

Synonyms:hydrazon obtained by condensation of 2-pyridylhydrazine with p-methoxyacetophenone

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Chemical Property of hydrazon obtained by condensation of 2-pyridylhydrazine with p-methoxyacetophenone

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Technology Process of hydrazon obtained by condensation of 2-pyridylhydrazine with p-methoxyacetophenone

There total 3 articles about hydrazon obtained by condensation of 2-pyridylhydrazine with p-methoxyacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 4930-98-7
pyrid-2-ylhydrazine

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 82664-05-9
hydrazon obtained by condensation of 2-pyridylhydrazine with p-methoxyacetophenone

Guidance literature:: With hydrogenchloride; In ethanol; at 95 ℃; for 0.166667h; Microwave irradiation; Sealed tube;
DOI:10.1002/ejoc.201901178

Reference yield:

: 504-29-0
2-aminopyridine

: 82664-05-9
hydrazon obtained by condensation of 2-pyridylhydrazine with p-methoxyacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / 47percent HBr, Br₂, aq. NaCN / 0 °C

2: 54 percent / N₂H₄*H₂O / 4 h / Heating

3: 79 percent / 10percent HCl / ethanol / 2 h / Heating

With hydrogenchloride; sodium cyanide; hydrogen bromide; bromine; hydrazine hydrate; In ethanol;
DOI:10.1016/S0223-5234(98)80008-1

Reference yield:

: 109-04-6
2-bromo-pyridine

: 82664-05-9
hydrazon obtained by condensation of 2-pyridylhydrazine with p-methoxyacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / N₂H₄*H₂O / 4 h / Heating

2: 79 percent / 10percent HCl / ethanol / 2 h / Heating

With hydrogenchloride; hydrazine hydrate; In ethanol;
DOI:10.1016/S0223-5234(98)80008-1