(E)-3-Phenyl-acrylic acid 4-{(2-cyano-ethyl)-[(E)-(3-phenyl-acryloyl)]-amino}-butyl ester

Base Information

Chemical Name:(E)-3-Phenyl-acrylic acid 4-{(2-cyano-ethyl)-[(E)-(3-phenyl-acryloyl)]-amino}-butyl ester
CAS No.:107199-58-6
Molecular Formula:C₂₅H₂₆N₂O₃
Molecular Weight:402.493
Hs Code.:

Synonyms:(E)-3-Phenyl-acrylic acid 4-{(2-cyano-ethyl)-[(E)-(3-phenyl-acryloyl)]-amino}-butyl ester

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Chemical Property of (E)-3-Phenyl-acrylic acid 4-{(2-cyano-ethyl)-[(E)-(3-phenyl-acryloyl)]-amino}-butyl ester

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Technology Process of (E)-3-Phenyl-acrylic acid 4-{(2-cyano-ethyl)-[(E)-(3-phenyl-acryloyl)]-amino}-butyl ester

There total 1 articles about (E)-3-Phenyl-acrylic acid 4-{(2-cyano-ethyl)-[(E)-(3-phenyl-acryloyl)]-amino}-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107199-54-2
3-<(4-Hydroxybutyl)amino>propannitril

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 107199-58-6
(E)-3-Phenyl-acrylic acid 4-{(2-cyano-ethyl)-[(E)-(3-phenyl-acryloyl)]-amino}-butyl ester

Guidance literature:: DOI:10.1016/S0040-4039(00)83978-7

Reference yield: 90.0%

: 107199-58-6
(E)-3-Phenyl-acrylic acid 4-{(2-cyano-ethyl)-[(E)-(3-phenyl-acryloyl)]-amino}-butyl ester

: 107199-57-5
3-Phenyl-propionic acid 4-[(3-amino-propyl)-(3-phenyl-propionyl)-amino]-butyl ester

Guidance literature:: With hydrogen; platinum(IV) oxide;
DOI:10.1016/S0040-4039(00)83978-7

Reference yield:

: 107199-58-6
(E)-3-Phenyl-acrylic acid 4-{(2-cyano-ethyl)-[(E)-(3-phenyl-acryloyl)]-amino}-butyl ester

: 53938-06-0
(-)-dihydrocelacinnine

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / H₂ / platinum oxide

2: 80 percent / 2-chloro-1-methylpyridinium iodide

3: 90 percent / aq. K₂CO₃

4: 70 percent / pyridinium chlorochromate

5: 90 percent / trifluoroacetic acid

6: 1.) NaHCO₃ 2.) NaBH₄ / 1.) room temperature

With sodium tetrahydroborate; 2-chloro-1-methyl-pyridinium iodide; hydrogen; sodium hydrogencarbonate; potassium carbonate; pyridinium chlorochromate; trifluoroacetic acid; platinum(IV) oxide;
DOI:10.1016/S0040-4039(00)83978-7