N⁽⁶⁾-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylideneadenosine

Base Information

• Chemical Name: N⁽⁶⁾-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylideneadenosine
• CAS No.: 801316-89-2
• Molecular Formula: C₂₉H₄₁N₅O₆Si
• Molecular Weight: 583.76

Synonyms:N⁽⁶⁾-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylideneadenosine

Chemical Property of N⁽⁶⁾-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylideneadenosine

Chemical Property:

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Technology Process of N⁽⁶⁾-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylideneadenosine

There total 1 articles about N⁽⁶⁾-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylideneadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N6-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-formyl-2',3'-O-isopropylideneadenosine → N(6)-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylideneadenosine (801316-89-2)

Guidance literature:

With sodium tetrahydroborate; acetic acid; In tetrahydrofuran; ethanol; at 23 ℃; for 0.5h;

DOI:10.1002/hlca.200890071

Reference yield: 85.0%

Methanesulfonic anhydride (7143-01-3) + N(6)-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylideneadenosine (801316-89-2) → Methanesulfonic acid 6-benzoylamino-9-{(3aR,4R,6R,6aR)-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxymethyl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-9H-purin-8-ylmethyl ester (801316-91-6)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 1h;

DOI:10.1002/hlca.200490204

Reference yield: 83.0%

(4-methoxyphenyl)diphenylmethyl chloride + N(6)-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylideneadenosine (801316-89-2) → N(6)-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine (1040239-11-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 23 ℃; for 4.16667h; Inert atmosphere;

DOI:10.1002/hlca.200890071

Downstream raw materials:

Methanesulfonic acid 6-benzoylamino-9-{(3aR,4R,6R,6aR)-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxymethyl]-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl}-9H-purin-8-ylmethyl ester

N⁽⁶⁾-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine

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