(1S,3R,5S)-Cyclohexane-1,3,5-tricarboxylic acid bis-{[2-(2-hydroxy-ethoxy)-ethyl]-amide} [(S)-2-phenyl-1-(quinolin-6-ylcarbamoyl)-ethyl]-amide

Base Information

Chemical Name:(1S,3R,5S)-Cyclohexane-1,3,5-tricarboxylic acid bis-{[2-(2-hydroxy-ethoxy)-ethyl]-amide} [(S)-2-phenyl-1-(quinolin-6-ylcarbamoyl)-ethyl]-amide
CAS No.:800373-95-9
Molecular Formula:C₃₅H₄₅N₅O₈
Molecular Weight:663.771
Hs Code.:

Synonyms:(1S,3R,5S)-Cyclohexane-1,3,5-tricarboxylic acid bis-{[2-(2-hydroxy-ethoxy)-ethyl]-amide} [(S)-2-phenyl-1-(quinolin-6-ylcarbamoyl)-ethyl]-amide

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Chemical Property of (1S,3R,5S)-Cyclohexane-1,3,5-tricarboxylic acid bis-{[2-(2-hydroxy-ethoxy)-ethyl]-amide} [(S)-2-phenyl-1-(quinolin-6-ylcarbamoyl)-ethyl]-amide

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Technology Process of (1S,3R,5S)-Cyclohexane-1,3,5-tricarboxylic acid bis-{[2-(2-hydroxy-ethoxy)-ethyl]-amide} [(S)-2-phenyl-1-(quinolin-6-ylcarbamoyl)-ethyl]-amide

There total 4 articles about (1S,3R,5S)-Cyclohexane-1,3,5-tricarboxylic acid bis-{[2-(2-hydroxy-ethoxy)-ethyl]-amide} [(S)-2-phenyl-1-(quinolin-6-ylcarbamoyl)-ethyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.1%

: 800373-98-2
(1R,3S,5R)-5-[(S)-2-Phenyl-1-(quinolin-6-ylcarbamoyl)-ethylcarbamoyl]-cyclohexane-1,3-dicarboxylic acid

: 929-06-6
2-(2-Aminoethoxy)ethanol

: 800373-95-9
(1S,3R,5S)-Cyclohexane-1,3,5-tricarboxylic acid bis-{[2-(2-hydroxy-ethoxy)-ethyl]-amide} [(S)-2-phenyl-1-(quinolin-6-ylcarbamoyl)-ethyl]-amide

Guidance literature:: With 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In methanol; dimethyl sulfoxide; at 20 ℃;
DOI:10.1039/b507157g

Reference yield: 42.1%

: 800373-95-9
(1S,3R,5S)-Cyclohexane-1,3,5-tricarboxylic acid bis-{[2-(2-hydroxy-ethoxy)-ethyl]-amide} [(S)-2-phenyl-1-(quinolin-6-ylcarbamoyl)-ethyl]-amide

Guidance literature:

Reference yield:

: 2-amino-3-phenyl-N-quinolin-6-yl-propionamide; compound with GENERIC INORGANIC NEUTRAL COMPONENT

: 800373-95-9
(1S,3R,5S)-Cyclohexane-1,3,5-tricarboxylic acid bis-{[2-(2-hydroxy-ethoxy)-ethyl]-amide} [(S)-2-phenyl-1-(quinolin-6-ylcarbamoyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: HOBT; CDI / dimethylsulfoxide / 2 h / 20 °C

1.2: 60.3 percent / Et₃N / dimethylsulfoxide

2.1: 42.1 percent / DMT-MM / methanol; dimethylsulfoxide / 20 °C

With benzotriazol-1-ol; 1,1'-carbonyldiimidazole; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride; In methanol; dimethyl sulfoxide;
DOI:10.1039/b507157g