(S)-3-((4S,5S)-4,5-Bis-methoxymethyl-2-phenyl-[1,3]dioxolan-2-yl)-butane-1,3-diol

Base Information

Chemical Name:(S)-3-((4S,5S)-4,5-Bis-methoxymethyl-2-phenyl-[1,3]dioxolan-2-yl)-butane-1,3-diol
CAS No.:108031-41-0
Molecular Formula:C₁₇H₂₆O₆
Molecular Weight:326.39
Hs Code.:

Synonyms:(S)-3-((4S,5S)-4,5-Bis-methoxymethyl-2-phenyl-[1,3]dioxolan-2-yl)-butane-1,3-diol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-3-((4S,5S)-4,5-Bis-methoxymethyl-2-phenyl-[1,3]dioxolan-2-yl)-butane-1,3-diol

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Technology Process of (S)-3-((4S,5S)-4,5-Bis-methoxymethyl-2-phenyl-[1,3]dioxolan-2-yl)-butane-1,3-diol

There total 8 articles about (S)-3-((4S,5S)-4,5-Bis-methoxymethyl-2-phenyl-[1,3]dioxolan-2-yl)-butane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107954-37-0
(S)-2-((4S,5S)-4,5-Bis-methoxymethyl-2-phenyl-[1,3]dioxolan-2-yl)-but-3-yn-2-ol

: 108031-41-0
(S)-3-((4S,5S)-4,5-Bis-methoxymethyl-2-phenyl-[1,3]dioxolan-2-yl)-butane-1,3-diol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 5percent Pd/C / ethyl acetate / Ambient temperature

2: 1.) B₂H₆, 2.) 30percent H₂O₂, 3M NaOH / 1.) THF, 0 deg C, RT_., 40 min. 2.) 40 deg C, 1 h

With sodium hydroxide; hydrogen; dihydrogen peroxide; diborane; palladium on activated charcoal; In ethyl acetate;

Reference yield:

: 107968-18-3,107968-19-4
2-((4S,5S)-4,5-Bis-methoxymethyl-2-phenyl-[1,3]dioxolan-2-yl)-4-trimethylsilanyl-but-3-yn-2-ol

: 108031-41-0
(S)-3-((4S,5S)-4,5-Bis-methoxymethyl-2-phenyl-[1,3]dioxolan-2-yl)-butane-1,3-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / 0.5percent KOH / aq. ethanol / 0.25 h / Heating

2: H₂ / 5percent Pd/C / ethyl acetate / Ambient temperature

3: 1.) B₂H₆, 2.) 30percent H₂O₂, 3M NaOH / 1.) THF, 0 deg C, RT_., 40 min. 2.) 40 deg C, 1 h

With potassium hydroxide; sodium hydroxide; hydrogen; dihydrogen peroxide; diborane; palladium on activated charcoal; In ethanol; ethyl acetate;

Reference yield:

: 50622-10-1
(-)-(2S,3S)-1,4-dimethoxy-2,3-butanediol

: 108031-41-0
(S)-3-((4S,5S)-4,5-Bis-methoxymethyl-2-phenyl-[1,3]dioxolan-2-yl)-butane-1,3-diol

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / CSA / Ambient temperature

2: 98 percent / (COCl)2,DMSO, Et₃N / CH₂Cl₂ / 0.5 h / -78 °C

3: tetrahydrofuran / -78 °C

4: 1.) B₂H₆, 2.) 30percent H₂O₂, 3M NaOH / 1.) THF, 0 deg C, RT_., 40 min. 2.) 40 deg C, 1 h

With sodium hydroxide; oxalyl dichloride; camphor-10-sulfonic acid; dihydrogen peroxide; dimethyl sulfoxide; triethylamine; diborane; In tetrahydrofuran; dichloromethane;