Technology Process of 2-iodo-4-benzyloxyindan
There total 7 articles about 2-iodo-4-benzyloxyindan which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium iodide;
In
acetone;
Yield given;
Heating;
DOI:10.1021/ja00353a024
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 100 percent / potassium carbonate / acetone / 4 h / Heating
2: 91 percent / sulfuric acid / methanol / 3 h / Heating
3: 70 percent / n-butyllithium / tetrahydrofuran; hexane / 48 h / Ambient temperature
4: 1.) borane-methyl sulfide complex, 2.) hydrogen peroxide, sodium hydroxide / 1.) THF, room temperature, 3 h, 2.) water, 25 deg C; reflux, 1 h
6: sodium iodide / acetone / Heating
With
sodium hydroxide; n-butyllithium; dimethylsulfide borane complex; sulfuric acid; dihydrogen peroxide; potassium carbonate; sodium iodide;
In
tetrahydrofuran; methanol; hexane; acetone;
DOI:10.1021/ja00353a024
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 100 percent / potassium carbonate / acetone / 4 h / Heating
2: 91 percent / sulfuric acid / methanol / 3 h / Heating
3: 70 percent / n-butyllithium / tetrahydrofuran; hexane / 48 h / Ambient temperature
4: 1.) borane-methyl sulfide complex, 2.) hydrogen peroxide, sodium hydroxide / 1.) THF, room temperature, 3 h, 2.) water, 25 deg C; reflux, 1 h
6: sodium iodide / acetone / Heating
With
sodium hydroxide; n-butyllithium; dimethylsulfide borane complex; sulfuric acid; dihydrogen peroxide; potassium carbonate; sodium iodide;
In
tetrahydrofuran; methanol; hexane; acetone;
DOI:10.1021/ja00353a024
