benzyl 4'-O-benzoyl-2,3,6,2',6'-penta-O-(4-chlorobenzoyl)-β-D-lactoside

Base Information

Chemical Name:benzyl 4'-O-benzoyl-2,3,6,2',6'-penta-O-(4-chlorobenzoyl)-β-D-lactoside
CAS No.:1329426-47-2
Molecular Formula:C₆₁H₄₇Cl₅O₁₇
Molecular Weight:1229.3
Hs Code.:

Synonyms:benzyl 4'-O-benzoyl-2,3,6,2',6'-penta-O-(4-chlorobenzoyl)-β-D-lactoside

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Chemical Property of benzyl 4'-O-benzoyl-2,3,6,2',6'-penta-O-(4-chlorobenzoyl)-β-D-lactoside

Chemical Property:

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Technology Process of benzyl 4'-O-benzoyl-2,3,6,2',6'-penta-O-(4-chlorobenzoyl)-β-D-lactoside

There total 4 articles about benzyl 4'-O-benzoyl-2,3,6,2',6'-penta-O-(4-chlorobenzoyl)-β-D-lactoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1329426-42-7
benzyl 2,3,6,2′,6′-penta-O-(4-chlorobenzoyl)-β-D-lactoside

: 707-07-3
orthobenzoic acid trimethyl ester

: 1329426-47-2
benzyl 4'-O-benzoyl-2,3,6,2',6'-penta-O-(4-chlorobenzoyl)-β-D-lactoside

Guidance literature:: benzyl 2,3,6,2′,6′-penta-O-(4-chlorobenzoyl)-β-D-lactoside; orthobenzoic acid trimethyl ester; In toluene; at 20 ℃; for 3h;

With acetic acid; In toluene; for 1h;

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 1329426-47-2
benzyl 4'-O-benzoyl-2,3,6,2',6'-penta-O-(4-chlorobenzoyl)-β-D-lactoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloro-trimethyl-silane / acetone / 5 h / 20 °C

1.2: 40 - 45 °C

2.1: perchloric acid / dichloromethane; acetonitrile; water / 0.5 h / 20 °C

3.1: camphenesulphonic acid / toluene / 3 h / 20 °C

3.2: 1 h

With chloro-trimethyl-silane; perchloric acid; In dichloromethane; water; acetone; toluene; acetonitrile;

Reference yield:

: 18404-72-3
benzyl 4-O-β-D-galactopyranosyl-β-D-glucopyranoside

: 1329426-47-2
benzyl 4'-O-benzoyl-2,3,6,2',6'-penta-O-(4-chlorobenzoyl)-β-D-lactoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: chloro-trimethyl-silane / acetone / 5 h / 20 °C

1.2: 40 - 45 °C

2.1: perchloric acid / dichloromethane; acetonitrile; water / 0.5 h / 20 °C

3.1: camphenesulphonic acid / toluene / 3 h / 20 °C

3.2: 1 h

With chloro-trimethyl-silane; perchloric acid; In dichloromethane; water; acetone; toluene; acetonitrile;