(S)-2-[(S)-2-(Benzyloxycarbonyl-methyl-amino)-3-phenyl-propionylamino]-3-(1H-imidazol-4-yl)-propionic acid methyl ester

Base Information

Chemical Name:(S)-2-[(S)-2-(Benzyloxycarbonyl-methyl-amino)-3-phenyl-propionylamino]-3-(1H-imidazol-4-yl)-propionic acid methyl ester
CAS No.:192064-88-3
Molecular Formula:C₂₅H₂₈N₄O₅
Molecular Weight:464.521
Hs Code.:

Synonyms:(S)-2-[(S)-2-(Benzyloxycarbonyl-methyl-amino)-3-phenyl-propionylamino]-3-(1H-imidazol-4-yl)-propionic acid methyl ester

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Chemical Property of (S)-2-[(S)-2-(Benzyloxycarbonyl-methyl-amino)-3-phenyl-propionylamino]-3-(1H-imidazol-4-yl)-propionic acid methyl ester

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Technology Process of (S)-2-[(S)-2-(Benzyloxycarbonyl-methyl-amino)-3-phenyl-propionylamino]-3-(1H-imidazol-4-yl)-propionic acid methyl ester

There total 1 articles about (S)-2-[(S)-2-(Benzyloxycarbonyl-methyl-amino)-3-phenyl-propionylamino]-3-(1H-imidazol-4-yl)-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 2899-07-2
(S)-N-benzyloxycarbonyl-N-methyl-phenyl alanine

: 4467-54-3,5619-10-3,7389-87-9,18684-16-7,22888-60-4,32381-17-2,92742-29-5,100009-20-9
l-histidine methyl ester dihydrochloride

: 192064-88-3
(S)-2-[(S)-2-(Benzyloxycarbonyl-methyl-amino)-3-phenyl-propionylamino]-3-(1H-imidazol-4-yl)-propionic acid methyl ester

Guidance literature:: With triethylamine; isobutyl chloroformate; In tetrahydrofuran; 1) 0 deg C, 90 min, 2) to r.t., 12 h;
DOI:10.1007/BF00807896

Reference yield:

: 192064-88-3
(S)-2-[(S)-2-(Benzyloxycarbonyl-methyl-amino)-3-phenyl-propionylamino]-3-(1H-imidazol-4-yl)-propionic acid methyl ester

: 143072-03-1
N-methyl-L-phenylalanyl-L-histidine methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 6h; under 3800 Torr; Ambient temperature;
DOI:10.1007/BF00807896

Reference yield:

: 192064-88-3
(S)-2-[(S)-2-(Benzyloxycarbonyl-methyl-amino)-3-phenyl-propionylamino]-3-(1H-imidazol-4-yl)-propionic acid methyl ester

: cyclo

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd-C / methanol / 6 h / 3800 Torr / Ambient temperature

2: 2 h / 110 - 120 °C / 0.01 Torr

With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1007/BF00807896