1,10,19,28-tetra<4-(acetylthio)benzoyl>-1,10,19,28-tetra-azacyclohexatriacontane

Base Information

Chemical Name:1,10,19,28-tetra<4-(acetylthio)benzoyl>-1,10,19,28-tetra-azacyclohexatriacontane
CAS No.:132035-66-6
Molecular Formula:C₆₈H₉₂N₄O₈S₄
Molecular Weight:1221.76
Hs Code.:

Synonyms:1,10,19,28-tetra<4-(acetylthio)benzoyl>-1,10,19,28-tetra-azacyclohexatriacontane

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Chemical Property of 1,10,19,28-tetra<4-(acetylthio)benzoyl>-1,10,19,28-tetra-azacyclohexatriacontane

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Technology Process of 1,10,19,28-tetra<4-(acetylthio)benzoyl>-1,10,19,28-tetra-azacyclohexatriacontane

There total 4 articles about 1,10,19,28-tetra<4-(acetylthio)benzoyl>-1,10,19,28-tetra-azacyclohexatriacontane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 129018-26-4
thioacetic acid S-(4-chlorocarbonyl-phenyl) ester

: 129688-00-2
1,10,19,28-Tetraaza-cyclohexatriacontane; hydrochloride

: 132035-66-6
1,10,19,28-tetra<4-(acetylthio)benzoyl>-1,10,19,28-tetra-azacyclohexatriacontane

Guidance literature:: With triethylamine; In dichloromethane; for 2.5h; Ambient temperature;
DOI:10.1039/DT9900003375

Reference yield:

: 1074-36-8
4-mercaptobenzoic acid

: 132035-66-6
1,10,19,28-tetra<4-(acetylthio)benzoyl>-1,10,19,28-tetra-azacyclohexatriacontane

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / pyridine

2: 80 percent / oxalyl chloride / benzene / 1 h / Heating

3: 89 percent / Et₃N / CH₂Cl₂ / 2.5 h / Ambient temperature

With pyridine; oxalyl dichloride; triethylamine; In dichloromethane; benzene;
DOI:10.1039/DT9900003375

Reference yield:

: 24197-62-4
S-acetyl-4-mercaptobenzoic acid

: 132035-66-6
1,10,19,28-tetra<4-(acetylthio)benzoyl>-1,10,19,28-tetra-azacyclohexatriacontane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / oxalyl chloride / benzene / 1 h / Heating

2: 89 percent / Et₃N / CH₂Cl₂ / 2.5 h / Ambient temperature

With oxalyl dichloride; triethylamine; In dichloromethane; benzene;
DOI:10.1039/DT9900003375