Ethan-1,2-bis-iodid

Base Information

• Chemical Name: Ethan-1,2-bis-iodid
• CAS No.: 16001-94-8
• Molecular Formula: C₂₈H₃₀P₂*2I
• Molecular Weight: 682.303

Synonyms:Ethan-1,2-bis-iodid

Chemical Property of Ethan-1,2-bis-iodid

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Technology Process of Ethan-1,2-bis-iodid

There total 10 articles about Ethan-1,2-bis-iodid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

methyl iodide (74-88-4) → Ethan-1,2-bis-iodid (16001-94-8)

Guidance literature:

With oct-1-ene; In tetrahydrofuran; Heating;

DOI:10.1016/S0040-4039(97)00647-3

Reference yield:

1,2-bis-(diphenylphosphino)ethane (1663-45-2) + methyl iodide (74-88-4) → Ethan-1,2-bis-iodid (16001-94-8)

Guidance literature:

In d⁽⁴⁾-methanol; at 55 ℃; for 2h; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.ica.2015.04.003

Reference yield:

1,2-bis-(diphenylphosphino)ethane (1663-45-2) + methyl iodide (74-88-4) → C27H27P2(1+)*I(1-) + Ethan-1,2-bis-iodid (16001-94-8)

Guidance literature:

In chloroform-d1; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.ica.2015.04.003

upstream raw materials:

(2-Iodethyl)phenylcarbonat

diphenyl(methyl)phosphine

1,2-Bis(diphenylphosphino)-1-(methyldiphenylphosphino)ethaniodid

methyl iodide

Downstream raw materials:

(C₆H₅)2P(CH₃)CH₂CH₂P(CH₃)(C₆H₅)2⁽²⁺⁾*InI₃^(2-)=[(C₆H₅)2P(CH₃)CH₂CH₂P(CH₃)(C₆H₅)2][InI₃]

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