ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate

Base Information

Chemical Name:ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate
CAS No.:82585-73-7
Molecular Formula:C₁₈H₂₂N₆O₅
Molecular Weight:402.41
Hs Code.:

Synonyms:ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate

There total 2 articles about ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 82585-86-2
ethyl 6-amino-4-<<2-hydroxy-3-(N-methyl-N-phenylamino)propyl>amino>-5-nitro-2-pyridinecarbamate

: 82585-73-7
ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate

Guidance literature:: With phosphoric acid; dimethyl sulfoxide; dicyclohexyl-carbodiimide; at 25 ℃; for 2.5h;
DOI:10.1021/jm00351a008

Reference yield:

: 63062-22-6
3-(N-Methyl-N-phenylamino)-2-hydroxypropylamine

: 82585-73-7
ethyl 6-amino-4-<<3-(N-methyl-N-phenylamino)-2-oxopropyl>amino>-5-nitro-2-pyridinecarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Et₃N / methanol / 18 h / 60 °C

2: 80 percent / orthophosphoric acid, DCC, DMSO / 2.5 h / 25 °C

With phosphoric acid; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; In methanol;
DOI:10.1021/jm00351a008